Mass Spectrometry of Polymers PDF Download

Author: Giorgio Montaudo
Publisher: CRC Press
ISBN: 1420037757
Category : Science
Languages : en
Pages : 601

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Book Description
Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results

Author: Minna Hakkarainen
Publisher: Springer Science & Business Media
ISBN: 3642280404
Category : Technology & Engineering
Languages : en
Pages : 219

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Book Description
Emerging Mass Spectrometric Tools for Analysis of Polymers and Polymer Additives, by Nina Aminlashgari and Minna Hakkarainen. Analysis of Polymer Additives and Impurities by Liquid Chromatography/Mass Spectrometry and Capillary Electrophoresis/Mass Spectrometry, by Wolfgang Buchberger and Martin Stiftinger. Direct Insertion Probe Mass Spectrometry of Polymers, by Jale Hacaloglu Mass Spectrometric Characterization of Oligo- and Polysaccharides and Their Derivatives, by Petra Mischnick. Electrospray Ionization-Mass Spectrometry for Molecular Level Understanding of Polymer Degradation, by Minna Hakkarainen.

Author: Christopher Barner-Kowollik
Publisher: John Wiley & Sons
ISBN: 3527641831
Category : Science
Languages : en
Pages : 501

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Book Description
Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.

Author: Muhammad Imran Malik
Publisher: Elsevier
ISBN: 012822598X
Category : Technology & Engineering
Languages : en
Pages : 670

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Book Description
Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. - Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity - Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material - Establishes a strong link between basic principles, characterization techniques, and real-life applications

Author: J.L. Koenig
Publisher: Elsevier
ISBN: 0080541577
Category : Technology & Engineering
Languages : en
Pages : 509

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Book Description
This revised and updated Second Edition of the best-selling reference/text is essential reading for students and scientists who seek a thorough and practical introduction to the field of polymer spectroscopy. Eleven chapters cover the fundamental aspects and experimental applications of the primary spectroscopic methods. The advantages and disadvantages of the various techniques for particular polymer systems are also discussed. The goal of the author is not to make the reader an expert in the field, but rather to provide enough information about the different spectroscopic methods that the reader can determine how the available techniques can be used to solve a particular polymer problem. This Second Edition contains new and updated information on techniques in IR and NMR, as well as an all-new chapter on Mass Spectrometry.

Author: Shin Tsuge
Publisher: Elsevier
ISBN: 0444538933
Category : Science
Languages : en
Pages : 405

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Book Description
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample

Author: Harald Pasch
Publisher: Springer Science & Business Media
ISBN: 9783540442592
Category : Science
Languages : en
Pages : 334

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Book Description
MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.

Author: Rui Yang
Publisher: CRC Press
ISBN: 135121313X
Category : Science
Languages : en
Pages : 287

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Book Description
Analytical Methods for Polymer Characterization presents a collection of methods for polymer analysis. Topics include chromatographic methods (gas chromatography, inverse gas chromatography, and pyrolysis gas chromatography), mass spectrometry, spectroscopic methods (ultraviolet-visible spectroscopy, infrared spectroscopy, Raman spectroscopy, and nuclear magnetic resonance), thermal analysis (differential scanning calorimetry and thermogravimetry), microscopy methods (scanning electron microscopy, transmission electron microscopy, and atomic force microscopy), and x-ray diffraction. The author also discusses mechanical and dynamic mechanical properties.

Author: Jyotishkumar Parameswaranpillai
Publisher: John Wiley & Sons
ISBN: 3527346481
Category : Technology & Engineering
Languages : en
Pages : 402

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Book Description
State-of-the-art overview on bioepoxy polymers as well as their blends and composites -- covering all aspects from fundamentals to applications! Bioepoxy polymers is an emerging area and have attracted more and more attention due to their biodegradability and good thermo-mechanical performance. In recent years, research progress has been made in synthesis, processing, characterization, and applications of bioepoxy blends and composites. Bioepoxy polymers are very promising candidates to replace the traditional thermosetting nonbiodegradable polymers. Bio-Based Epoxy Polymers, Blends and Composites summaries recent research progress on bioepoxy polymers as well as their blends and composites. It covers aspects from synthesis, processing, various characterization techniques to broad spectrum of applications. It provides a correlation of physical properties with macro, micro and nanostructures of the materials. Moreover, research trends, future directions, and opportunities are also discussed. Attracts attention: Bioepoxy polymers are environmentally friendly and considered as a promising candidate to replace the traditional thermosetting nonbiodegradable polymers Highly application-oriented: Bioepoxy polymers can be used in a broad range of applications such as polymer foams, construction, aerospace, automobiles, self-healing systems One-stop reference: Covers all aspects of bioepoxy polymer, their blends and composites, such as synthesis, properties, processing, characterization and applications Broad audience: Attracts attention from both academia and industry

Author: Charles E. Carraher Jr.
Publisher: CRC Press
ISBN: 1466552204
Category : Science
Languages : en
Pages : 794

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Book Description
Most of the advancements in communication, computers, medicine, and air and water purity are linked to macromolecules and a fundamental understanding of the principles that govern their behavior. These fundamentals are explored in Carraher's Polymer Chemistry, Ninth Edition. Continuing the tradition of previous volumes, the latest edition provides a well-rounded presentation of the principles and applications of polymers. With an emphasis on the environment and green chemistry and materials, this edition offers detailed coverage of natural and synthetic giant molecules, inorganic and organic polymers, biomacromolecules, elastomers, adhesives, coatings, fibers, plastics, blends, caulks, composites, and ceramics. Using simple fundamentals, this book demonstrates how the basic principles of one polymer group can be applied to all of the other groups. It covers reactivities, synthesis and polymerization reactions, techniques for characterization and analysis, energy absorption and thermal conductivity, physical and optical properties, and practical applications. This edition includes updated techniques, new sections on a number of copolymers, expanded emphasis on nanotechnology and nanomaterials, and increased coverage of topics including carbon nanotubes, tapes and glues, photochemistry, and more. With topics presented so students can understand polymer science even if certain parts of the text are skipped, this book is suitable as an undergraduate as well as an introductory graduate-level text. The author begins most chapters with theory followed by application, and generally addresses the most critical topics first. He provides all of the elements of an introductory text, covering synthesis, properties, applications, and characterization. This user-friendly book also contains definitions, learning objectives, questions, and additional reading in each chapter.