Inorganic Thermogravimetric Analysis PDF Download

Author: Clément Duval
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 750

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Author: David L. Bish
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 210

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Precision scanning calorimetry of clay minerals nad their intercalates; High-pressure differential thermal analysis: applications to clay minerals; Thermogravimetric analysis of minerals; Vacuum thermogravimetric analysis ans evolved gas analysis by mass spectrometry.

Author: Bernhard Wunderlich
Publisher: Springer Science & Business Media
ISBN: 9783540236290
Category : Science
Languages : en
Pages : 918

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Table of Contents Table of Contents 1 Atoms, small, and large molecules 2 Basics of thermal analysis 3 Dynamics of chemical and phase changes 4 Thermal analysis tools 5 Structure and properties of materials 6 Single component materials 7 Multiple component materials App. A.1 Table of thermal properties of linear macromolecules and related small molecules - the ATHAS data bank App. A.2 Radiation scattering App. A.3 Derivation of the Rayleigh ratio App. A.4 Neural network predictions App. A.5 Legendre transformations, Maxwell relations, linking of entropy and probability, and derivation of (dS/dT) App. A.6 Boltzmann distribution, harmonic vibration, complex numbers, and normal modes App. A.7 Summary of the basic kinetics of chemical reactions App. A.8 The ITS 1990 and the Krypton-86 length standard App. A.9 Development of classical DTA to DSC App. A.10 Examples of DTA and DSC under extreme conditions App. A.11 Description of an online correction of the heat-flow rate App. A.12 Derivation of the heat-flow equations App. A.13 Description of sawtooth-modulation response App. A.14 An introduction to group theory, definitions of configurations and conformations, and a summary of rational and irrational numbers App. A.15 Summary of birefringence and polarizing microscopy App. A.16 Summary of X-ray diffraction and interference effects App. A.17 Optical analog of electron double diffraction to produce Moire patterns.

Author: Paul Gabbott
Publisher: John Wiley & Sons
ISBN: 0470698128
Category : Science
Languages : en
Pages : 480

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Book Description
Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Author: Satinder Ahuja
Publisher: Academic Press
ISBN: 9780120449828
Category : Medical
Languages : en
Pages : 444

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The United States Food and Drug Administration (FDA) and other regulatory bodies around the world require that impurities in drug substance and drug product levels recommended by the International Conference on Harmonisation (ICH) be isolated and characterized. Identifying process-related impurities and degradation products also helps us to understand the production of impurities and assists in defining degradation mechanisms. When this process is performed at an early stage, there is ample time to address various aspects of drug development to prevent or control the production of impurities and degradation products well before the regulatory filing and thus assure production of a high-quality drug product. This book, therefore, has been designed to meet the need for a reference text on the complex process of isolation and characterization of process-related (synthesis and formulation) impurities and degradation products to meet critical requlatory requirements. It's objective is to provide guidance on isolating and characterizing impurities of pharmaceuticals such as drug candidates, drug substances, and drug products. The book outlines impurity identification processes and will be a key resource document for impurity analysis, isolation/synthesis, and characterization. - Provides valuable information on isolation and characterization of impurities. - Gives a regulatory perspective on the subject. - Describes various considerations involved in meeting regulatory requirements. - Discusses various sources of impurities and degredation products.

Author: M.E. Brown
Publisher: Springer Science & Business Media
ISBN: 0306484048
Category : Technology & Engineering
Languages : en
Pages : 268

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to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.

Author: Robert F. Jr. Schwenker
Publisher: Elsevier
ISBN: 0323142796
Category : Technology & Engineering
Languages : en
Pages : 742

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Book Description
Thermal Analysis, Volume 1: Instrumentation, Organic Materials, and Polymers is a collection of papers presented at the Second International Conference on Thermal Analysis, held in Holy Cross College, Worcester, Massachusetts on August 18-23, 1968. The papers highlight a wide range of applications, from fundamental thermodynamics and kinetics to industrial process development. This book is divided into two major sections encompassing 45 chapters. The first section emphasizes the developments in the instrumentation aspects of thermal analysis. This section deals first with the developments of thermal analysis equipment, methods, and their corresponding application to various fields, including in pharmaceutical research. This section also examines the technique of differential thermal analysis, microcalorimetry, thermogravimetry, mass spectrometry, pyrolysis-flame detection, and thermal volatilization analysis. The second section explores the application of thermal analysis to organic materials, such as polymers and elastomer systems. This section specifically looks into the potential of differential thermal analysis, thermogravimetry, and time-of-flight mass spectrometry in analysis of specific organic materials. Measurements of electrical conductivity, magnetic, dielectric, photoelectric, thermodynamic, and thermophysical properties are also provided.

Author: ASM International
Publisher: ASM International
ISBN: 1615030735
Category : Technology & Engineering
Languages : en
Pages : 486

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The selection and application of engineered materials is an integrated process that requires an understanding of the interaction between materials properties, manufacturing characteristics, design considerations, and the total life cycle of the product. This reference book on engineering plastics provides practical and comprehensive coverage on how the performance of plastics is characterized during design, property testing, and failure analysis. The fundamental structure and properties of plastics are reviewed for general reference, and detailed articles describe the important design factors, properties, and failure mechanisms of plastics. The effects of composition, processing, and structure are detailed in articles on the physical, chemical, thermal, and mechanical properties. Other articles cover failure mechanisms such as: crazing and fracture; impact loading; fatigue failure; wear failures, moisture related failure; organic chemical related failure; photolytic degradation; and microbial degradation. Characterization of plastics in failure analysis is described with additional articles on analysis of structure, surface analysis, and fractography.

Author: I. M. Kolthoff
Publisher: John Wiley & Sons
ISBN: 9780471806479
Category : Science
Languages : en
Pages : 438

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Book Description
A complete handbook for analytical chemists which has been designed to stimulate fundamental research. The contributors cover aspects of both classical and modern analytical chemistry, as well as the scientific and instrumental fundamentals of analytical methods.

Author: Charles Mansfield Earnest
Publisher: ASTM International
ISBN: 0803111770
Category : Composite materials
Languages : en
Pages : 298

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