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Author: G. Schlemmer Publisher: Birkhäuser ISBN: 3034875762 Category : Science Languages : en Pages : 292
Book Description
"One should rather go horne and mesh a net than jump into the pond and dive far fishes" (Chinese proverb) Recognizing the precise analytical question and planning the analysis according ly is certainly the first prerequisite for successful trace and ultratrace determina tions. The second prerequisite is to select the method appropriate to the analyti cal specification. The method itself consists of a set of available tools. The third prerequisite is that analysts and operators know the methods weH enough to enjoy challenging themselves as weH as the methods and are rewarded by the joy of high-quality data, fast and economical results and the conviction of having the analytical job under control. This skill is known among analysts or operators working with an exciting new and sometimes complicated analytical technique but is gradually lost on ce a technique becomes "mature" and a routine tool. Unfortunately, laboratory managers often do not allow sufficient training time for their analysts and technicians for "routine" techniques and thus miss an opportunity for motivating their co-workers and obtaining the full benefit of the equipment. Graphite furnace atomic absorption spectrometry (AAS) is one of the mature analytical techniques wh ich is seen as a routine method in most laboratories. More than 10,000 furnaces are operated in elemental trace and ultratrace analy ses in laboratories around the world today.
Author: G. Schlemmer Publisher: Birkhäuser ISBN: 3034875762 Category : Science Languages : en Pages : 292
Book Description
"One should rather go horne and mesh a net than jump into the pond and dive far fishes" (Chinese proverb) Recognizing the precise analytical question and planning the analysis according ly is certainly the first prerequisite for successful trace and ultratrace determina tions. The second prerequisite is to select the method appropriate to the analyti cal specification. The method itself consists of a set of available tools. The third prerequisite is that analysts and operators know the methods weH enough to enjoy challenging themselves as weH as the methods and are rewarded by the joy of high-quality data, fast and economical results and the conviction of having the analytical job under control. This skill is known among analysts or operators working with an exciting new and sometimes complicated analytical technique but is gradually lost on ce a technique becomes "mature" and a routine tool. Unfortunately, laboratory managers often do not allow sufficient training time for their analysts and technicians for "routine" techniques and thus miss an opportunity for motivating their co-workers and obtaining the full benefit of the equipment. Graphite furnace atomic absorption spectrometry (AAS) is one of the mature analytical techniques wh ich is seen as a routine method in most laboratories. More than 10,000 furnaces are operated in elemental trace and ultratrace analy ses in laboratories around the world today.
Author: L Lajunen Publisher: Royal Society of Chemistry ISBN: 1847551904 Category : Science Languages : en Pages : 355
Book Description
This book describes both the theory of atomic spectroscopy and all the major atomic spectrometric techniques (AAS, Flame-AES, Plasma AES, AFS, and ICP-MS), including basic concepts, instrumentation and applications. Spectrochemical Analysis by Atomic Absorption and Emission is very wide in scope and will be extremely useful to both undergraduates and lecturers undertaking modern analytical chemistry courses. It contains many figures and tables which illuminate the text, covers various sample preparation methods and gives suggestions for further reading.
Author: Bernhard Welz Publisher: John Wiley & Sons ISBN: 3527606378 Category : Science Languages : en Pages : 296
Book Description
High-resolution continuum source atomic absorption spectrometry (HR-CS AAS) is the most revolutionary innovation since the introduction of AAS in 1955. Here, the authors provide the first complete and comprehensive discussion of HR-CS AAS and its application to the analysis of a variety of difficult matrices. Published just in time with the first commercial instrument available for this new technique, the book is a must for all those who want to know more about HR-CS AAS, and in particular for all future users. The advantages of the new technique over conventional line-source AAS are clearly demonstrated using practical examples and numerous figures, many in full color. HR-CS AAS is overcoming essentially all the remaining limitations of established AAS, particularly the notorious problem of accurate background measurement and correction. Using a continuum radiation source and a CCD array detector makes the spectral environment visible to several tenths of a nanometer on both sides of the analytical line, tremendously facilitating method development and elimination of interferences. Conceived as a supplement to the standard reference work on AAS by B. Welz and M. Sperling, this book does not repeat such fundamentals as the principles of atomizers or atomization mechanisms. Instead, it is strictly focused on new and additional information required to profit from HR-CS AAS. It presents characteristic concentration for flame atomization and characteristic mass data for electrothermal atomization for all elements, as well as listing numerous secondary lines of lower sensitivity for the determination of higher analyte concentrations. The highly resolved molecular absorption spectra of nitric, sulfuric and phosphoric acids, observed in an air-acetylene flame, which are depicted together with the atomic lines of all elements, make it possible to predict potential spectral interferences.
Author: Zeev B. Alfassi Publisher: Wiley-VCH ISBN: Category : Science Languages : en Pages : 632
Book Description
Determination of Trace Elements Edited by Zeev B. Alfassi The best way to determine trace elements! This easy-to-use handbook guides the reader through the maze of all modern analytical operations. Each method is described by an expert in the field. The book highlights the advantages and disadvantages of individual techniques and enables pharmacologists, environmentalists, material scientists, and food industry to select a judicious procedure for their trace element analysis.
Author: Ulrich Kurfürst Publisher: Springer Science & Business Media ISBN: 3662037165 Category : Science Languages : en Pages : 442
Book Description
The analysis of solid materials by introducing solid test sampies directly into the graphite furnace of an atomic absorption spectrometer must be regarded as a powerful analytical approach. Even if it is - of course - not the "ultimate method". After three decades of development, the instrumentation and the methodology are available to apply solid sampling successfully for the analysis of almost every material. Moreover, several tasks cannot be solved using other analytical methods as neatly as they can using direct solid sampling. The conventional methods work more or less satisfactorily, so why do we sug gest applying solid sampling much more extensively than it is today? To begin with, the features pointed out time and again should be named: Rapidity of the analytical procedure, low susceptibility to analyte loss or contamination, very smallquantities can be analyzed, and expenditure on instrumentation and per sonell is also low. These properties are examined and the necessary conditions are discussed (Chapter 1) as are the analytical tasks (Chapter 6) for which use of this method is advantageous. Other features that are often overlooked are just as important: The simplicity of the analytical procedures allows the analyst to main tain an intimate relationship with the original scientific task that has to be solved with the analysis. Furthermore, the considerable reduction of working place haz ards and pollution by avoiding the use of chemical reagents must nowadays be assessed as a feature as important as the others.
Author: A.J. (Tom) Van Loon Publisher: Elsevier ISBN: 0323154867 Category : Science Languages : en Pages : 350
Book Description
Analytical Atomic Absorption Spectroscopy presents the theories, methods, and principles in absorption spectrometry in an easily readable fashion that would suit the practicing analyst. The book covers the general principles involved in atomic spectroscopy, such as atomization and optical systems; electronic signal processing; and calibration procedures and accuracy and precision. The text then moves on to the preparation, determination, and analysis of different substances, such as waters, geological materials, metals and alloys, air samples, petroleum products, industrial samples, and metal compounds. The book also covers developments in the different areas of atomic spectroscopy, such as radiation sources, spectrometers, detectors, and other instruments. The text is recommended for practitioners and experts in the field of atomic spectroscopy, especially those looking for a book that details theories, practices, and advancements in the subject.
Author: G. Schlemmer Publisher: Springer Science & Business Media ISBN: 9783764357702 Category : Science Languages : en Pages : 300
Book Description
"One should rather go horne and mesh a net than jump into the pond and dive far fishes" (Chinese proverb) Recognizing the precise analytical question and planning the analysis according ly is certainly the first prerequisite for successful trace and ultratrace determina tions. The second prerequisite is to select the method appropriate to the analyti cal specification. The method itself consists of a set of available tools. The third prerequisite is that analysts and operators know the methods weH enough to enjoy challenging themselves as weH as the methods and are rewarded by the joy of high-quality data, fast and economical results and the conviction of having the analytical job under control. This skill is known among analysts or operators working with an exciting new and sometimes complicated analytical technique but is gradually lost on ce a technique becomes "mature" and a routine tool. Unfortunately, laboratory managers often do not allow sufficient training time for their analysts and technicians for "routine" techniques and thus miss an opportunity for motivating their co-workers and obtaining the full benefit of the equipment. Graphite furnace atomic absorption spectrometry (AAS) is one of the mature analytical techniques wh ich is seen as a routine method in most laboratories. More than 10,000 furnaces are operated in elemental trace and ultratrace analy ses in laboratories around the world today.
Author: L. Ebdon Publisher: John Wiley & Sons ISBN: 9780471974185 Category : Science Languages : en Pages : 212
Book Description
Das umfassende Handbuch der Atomspektroskopie jetzt in sorgfältig überarbeiteter, noch besser organisierter zweiter Auflage! Ergänzt wurden Kapitel zu wichtigen neuen Verfahren wie der Plasma-Atomemissionsspektroskopie und der ICP-Massenspektrometrie. Fettgedruckte Stichworte, übersichtliche Diagramme und praktische Übungen erleichtern das Erarbeiten und Vertiefen des Stoffes. (02/98)
Author: Maria Csuros Publisher: CRC Press ISBN: 1420032348 Category : Science Languages : en Pages : 405
Book Description
Determination of metals is a major part of the work of environmental testing laboratories. EPA and DEP methodology releases provide information only for selected areas of metals sampling and analysis, and their language makes them unsuitable for teaching and training purposes. Environmental Sampling and Analysis for Metals is a comprehensive and easy-to-read text for laboratory technicians and analytical chemists who need a guide for analyzing metals in environmental samples and a reference for analytical and quality control procedures.The book provides both theoretical and practical applications in metals analysis of environmental samples and incorporates the latest in analytical techniques, instrumentation, and regulations. Topics include sample collection, preservation, step-by-step analytical procedures, complete QA/QC requirements, data validation, and more. It also provides an overview of the occurrence, source, and fate of metallic substances in the environment, as well as their control by regulations and standards. Furthermore, the authors provide guidelines to help you prepare and understand reports. The analytical methods presented in Environmental Sampling and Analysis for Metals will be useful to anyone who produces, uses, or evaluates analytical data, and will be a valuable tool in environmental education and training programs.
Author: P.J. Potts Publisher: Springer Science & Business Media ISBN: 940153988X Category : Science Languages : en Pages : 633
Book Description
without an appreciation of what happens in between. The techniques available for the chemical analysis of silicate rocks have undergone a revolution over the last 30 years. However, to use an analytical technique most effectively, No longer is the analytical balance the only instrument used it is essential to understand its analytical characteristics, in for quantitative measurement, as it was in the days of classi particular the excitation mechanism and the response of the cal gravimetric procedures. A wide variety of instrumental signal detection system. In this book, these characteristics techniques is now commonly used for silicate rock analysis, have been described within a framework of practical ana lytical aplications, especially for the routine multi-element including some that incorporate excitation sources and detec tion systems that have been developed only in the last few analysis of silicate rocks. All analytical techniques available years. These instrumental developments now permit a wide for routine silicate rock analysis are discussed, including range of trace elements to be determined on a routine basis. some more specialized procedures. Sufficient detail is In parallel with these exciting advances, users have tended included to provide practitioners of geochemistry with a firm to become more remote from the data production process. base from which to assess current performance, and in some This is, in part, an inevitable result of the widespread intro cases, future developments.
Author: G. Schlemmer
Author: G. Schlemmer
Author: L Lajunen
Author: Bernhard Welz
Author: Zeev B. Alfassi
Author: Ulrich Kurfürst
Author: A.J. (Tom) Van Loon
Author: G. Schlemmer
Author: L. Ebdon
Author: Maria Csuros
Author: P.J. Potts