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Author: Paul Hagenmuller Publisher: Elsevier ISBN: 0323144365 Category : Science Languages : en Pages : 621
Book Description
Preparative Methods in Solid State Chemistry deals with the preparative methods used in solid state chemistry and highlights the importance of the chemist's role in preparing materials of desired quality as well as obtaining materials according to the requirements of the user such as the physicist. Topics covered range from high-pressure techniques in preparative chemistry to methods of growing single crystals of high-melting-point oxides. This book is comprised of 14 chapters and begins with an overview of possibilities for high-pressure synthesis, as well as the methods used to obtain high pressures, including transmission by gaseous or liquid fluids or in the solid state. The method of shock waves is then considered both from the point of view of thermodynamics and thermoelasticity, along with the possibility of using superpressures for evidently revolutionary applications. Subsequent chapters focus on the synthesis of single crystals of refractory oxides either at high temperatures (essentially liquid-solid transformations) or at lower temperatures in the presence of a solvent or a chemical reagent. The production of single crystals by electrolytic reduction in molten salts is also described. Numerous examples of vapor transport reactions in a temperature gradient are presented. This monograph should be of interest to chemists and students of solid state chemistry.
Author: Paul Hagenmuller Publisher: Elsevier ISBN: 0323144365 Category : Science Languages : en Pages : 621
Book Description
Preparative Methods in Solid State Chemistry deals with the preparative methods used in solid state chemistry and highlights the importance of the chemist's role in preparing materials of desired quality as well as obtaining materials according to the requirements of the user such as the physicist. Topics covered range from high-pressure techniques in preparative chemistry to methods of growing single crystals of high-melting-point oxides. This book is comprised of 14 chapters and begins with an overview of possibilities for high-pressure synthesis, as well as the methods used to obtain high pressures, including transmission by gaseous or liquid fluids or in the solid state. The method of shock waves is then considered both from the point of view of thermodynamics and thermoelasticity, along with the possibility of using superpressures for evidently revolutionary applications. Subsequent chapters focus on the synthesis of single crystals of refractory oxides either at high temperatures (essentially liquid-solid transformations) or at lower temperatures in the presence of a solvent or a chemical reagent. The production of single crystals by electrolytic reduction in molten salts is also described. Numerous examples of vapor transport reactions in a temperature gradient are presented. This monograph should be of interest to chemists and students of solid state chemistry.
Author: Riadh Marzouki Publisher: BoD – Books on Demand ISBN: 1838802231 Category : Technology & Engineering Languages : en Pages : 138
Book Description
New crystalline materials (organic, inorganic, hybrid) are promising for various applications, including electrical, piezoelectric, ferroelectric, magnetic, and catalytic processes. In addition, given their remarkable structural richness, these materials exhibit several interesting physical properties, such as ionic conduction, ion exchange, and others. Crystal growth, morphology, and grain size are factors influencing these physical properties. This book examines methods of synthesis of the most common crystalline materials and describes nucleation and crystal growth of various materials.
Author: Riadh Marzouki Publisher: ISBN: Category : Electronic books Languages : en Pages : 0
Book Description
The synthesis of single crystal is an area of intense activity in the materials science. The obtaining of the single crystal with sufficient dimension for X-ray diffraction depends on several factors including the chemical composition, crystal structure of the reagents, and physical parameters (temperature and pressure). In this context, this chapter is dedicated to the description of the most common synthesis methods of single crystal in the solid-state chemistry: solid-state method, hydrothermal, and slow evaporation at room temperature. Same other materials can be obtained at high pressure. There are also some physical techniques to grow single crystal, each technique is specific for specific materials.
Author: Aaron Wold Publisher: Springer Science & Business Media ISBN: 9401114765 Category : Science Languages : en Pages : 250
Book Description
The subject matterofsolid state chemistry lies within the spheres ofboth physical and inorganic chemistry. In addition, there is a large overlap with solid state physics and materials engineering. However, solid state chemistry has still to be recognized by the general body ofchemists as a legitimate subfield ofchemistry. The discipline is not even well defined as to content and has many facets that make writing a textbook a formidable task. The early studies carried out in the United States by Roland Ward and his co workers emphasized the synthesisofnew materials and the determination oftheir structure. His work on doped alkaline earth sulfides formed the basis for the development of infrared phosphors and his pioneering studies on oxides were important in understanding the structural features of both the perovskite oxides as well as the magnetoplumbites. In 1945, A. F. Wells published the first edition of Structural Inorganic Chemistry. This work attempts to demonstrate that the synthesis, structure, and properties of solids form an important part of inorganic chemistry. Now, after almost 50 years during which many notable advances have been made in solid state chemistry, it is still evident that the synthesis, structure determination, and properties of solids receive little attention in most treatments of inorganic chemistry. The development of the field since the early studies of Roland Ward (early 1940s) has been rapid.
Author: Richard Dronskowski Publisher: John Wiley & Sons ISBN: 3527325875 Category : Technology & Engineering Languages : en Pages : 3912
Book Description
This most comprehensive and unrivaled compendium in the field provides an up-to-date account of the chemistry of solids, nanoparticles and hybrid materials. Following a valuable introductory chapter reviewing important synthesis techniques, the handbook presents a series of contributions by about 150 international leading experts -- the "Who's Who" of solid state science. Clearly structured, in six volumes it collates the knowledge available on solid state chemistry, starting from the synthesis, and modern methods of structure determination. Understanding and measuring the physical properties of bulk solids and the theoretical basis of modern computational treatments of solids are given ample space, as are such modern trends as nanoparticles, surface properties and heterogeneous catalysis. Emphasis is placed throughout not only on the design and structure of solids but also on practical applications of these novel materials in real chemical situations.
Author: C. N. R. Rao Publisher: John Wiley & Sons ISBN: 111883254X Category : Science Languages : en Pages : 231
Book Description
This compact handbook describes all the important methods of synthesis employed today for synthesizing inorganic materials. Some features: Focuses on modern inorganic materials with applications in nanotechnology, energy materials, and sustainability Synthesis is a crucial component of materials science and technology; this book provides a simple introduction as well as an updated description of methods Written in a very simple style, providing references to the literature to get details of the methods of preparation when required
Author: A. K. Tyagi Publisher: Springer Nature ISBN: 9811618038 Category : Technology & Engineering Languages : en Pages : 856
Book Description
This book presents state-of-the-art coverage of synthesis of advanced functional materials. Unconventional synthetic routes play an important role in the synthesis of advanced materials as many new materials are metastable and cannot be synthesized by conventional methods. This book presents various synthesis methods such as conventional solid-state method, combustion method, a range of soft chemical methods, template synthesis, molecular precursor method, microwave synthesis, sono-chemical method and high-pressure synthesis. It provides a comprehensive overview of synthesis methods and covers a variety of materials, including ceramics, films, glass, carbon-based, and metallic materials. Many techniques for processing and surface functionalization are also discussed. Several engineering aspects of materials synthesis are also included. The contents of this book are useful for researchers and professionals working in the areas of materials and chemistry.
Author: Anthony R. West Publisher: John Wiley & Sons ISBN: 9780471908746 Category : Science Languages : en Pages : 752
Book Description
The first broad account offering a non-mathematical, unified treatment of solid state chemistry. Describes synthetic methods, X-ray diffraction, principles of inorganic crystal structures, crystal chemistry and bonding in solids; phase diagrams of 1, 2 and 3 component systems; the electrical, magnetic, and optical properties of solids; three groups of industrially important inorganic solids--glass, cement, and refractories; and certain aspects of organic solid state chemistry, including the ``organic metal'' of new materials.
Author: Paul Hagenmuller
Author: Paul Hagenmuller
Author: Riadh Marzouki
Author: Riadh Marzouki
Author: Patrick M. Woodward
Author: Aaron Wold
Author: Richard Dronskowski
Author: David Segal
Author: C. N. R. Rao
Author: A. K. Tyagi
Author: Anthony R. West