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Author: Helmut Duddeck Publisher: Springer Science & Business Media ISBN: 3642883109 Category : Science Languages : en Pages : 214
Book Description
During the last few years, routine applications of NMR (Nuclear Magnetic Resonance) techniques have developed at a tremendous pace. The latest generation of spectrometers have enabled chemists to perform new types of experiments, such as spinlock and inverse-detected methods. This third, revised and expanded edition introduces the latest methodologies and incorporates them into new exercises.
Author: Helmut Duddeck Publisher: Springer Science & Business Media ISBN: 3642883109 Category : Science Languages : en Pages : 214
Book Description
During the last few years, routine applications of NMR (Nuclear Magnetic Resonance) techniques have developed at a tremendous pace. The latest generation of spectrometers have enabled chemists to perform new types of experiments, such as spinlock and inverse-detected methods. This third, revised and expanded edition introduces the latest methodologies and incorporates them into new exercises.
Author: H. Duddeck Publisher: Springer Science & Business Media ISBN: 3642977812 Category : Science Languages : en Pages : 236
Book Description
For several years we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in the English version. This book could not have been written in the present form without the help of a number of col leagues and, therefore, we acknowledge gratefully the generous supply of samples from and useful discussions with B. Abegaz (Addis Ababa, Ethiopia), U.H. Brinker (Bingham, New York, USA), E.
Author: Antony J. Williams Publisher: Royal Society of Chemistry ISBN: 184973383X Category : Science Languages : en Pages : 344
Book Description
The first volume in a two-part set that discusses contemporary NMR approaches for the structure elucidation of natural products. It covers optimized hardware and experimental approaches.
Author: Antony Williams Publisher: Royal Society of Chemistry ISBN: 1849734682 Category : Science Languages : en Pages : 533
Book Description
The Ghanian plant Cryptolepis sanguinolenta is the source of a series of fascinating indoloquinoline alkaloids. The most unusual member of this alkaloid series was initially proposed to be a spiro nonacyclic structure, named cryptospirolepine, and was elucidated in 1993 based on the technologies available at that time. There were, however, several annoying attributes to the structure that bothered analysts for the ensuing 22 years. During the two decades that followed the initial work there have been enormous developments in NMR technology. Using new experimental approaches, specifically homodecoupled 1,1- and 1,n-HD-ADEQUATE NMR experiments developed in 2014, the structure of only a 700 μg sample of cryptospirolepine has been revised and is shown on the cover of this volume. The confluence of the NMR technological and methodological advances that allowed the revision of the structure of cryptospirolepine using a submilligram sample seems a fitting example for this book, which is dedicated to the NMR characterization of various classes of natural products. Volume 2 considers data processing and algorithmic based analyses tailored to natural product structure elucidation and reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, terpenes, steroids, alkaloids and carbohydrates. Volume 1 discusses contemporary NMR approaches including optimized and future hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. These books, bringing together acknowledged experts, uniquely focus on the combination of experimental approaches and modern hardware and software applied to the structure elucidation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products of pharmaceuticals that can be as scarce as natural product samples.
Author: Antony J. Williams Publisher: ISBN: 9781849733830 Category : Electronic book Languages : en Pages : 329
Book Description
The first volume in a two-part set that discusses contemporary NMR approaches for the structure elucidation of natural products. It covers optimized hardware and experimental approaches
Author: Antony J. Williams Publisher: ISBN: 9781849734592 Category : Science Languages : en Pages : 0
Book Description
This two volume set focuses on the structure elucidation of natural products forming an essential resource for spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products.
Author: Razvan Teodorescu Publisher: ISBN: Category : Languages : en Pages : 344
Book Description
The first volume in a two part set that discusses NMR analysis for the structure elucidation of natural products. It covers instrumentation for a contemporary laboratory and software.
Author: T. Claridge Publisher: Elsevier ISBN: 9780080427997 Category : Science Languages : en Pages : 408
Book Description
From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.
Author: Helmut Duddeck
Author: Helmut Duddeck
Author: H. Duddeck
Author: Antony J. Williams
Author: Antony Williams
Author: Springer
Author: Antony J. Williams
Author: Antony J. Williams
Author: Antony J. Williams
Author: Razvan Teodorescu
Author: T. Claridge