Selected Methods of Trace Metal Analysis PDF Download

Author: Jon Clement Van Loon
Publisher: Wiley-Interscience
ISBN:
Category : Science
Languages : en
Pages : 390

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Book Description
This monograph focuses on the analysis of trace metals in biological tissues and environmental materials. In most cases, procedures are so completely covered that no other source is necessary to finish an analysis. Includes chapters on such important topics as determination techniques, basic materials, sample preparation, botanical and zoological samples, and clinical samples.

Author: Zoltan Mester
Publisher: Elsevier
ISBN: 0080545483
Category : Science
Languages : en
Pages : 1339

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Book Description
Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation. - First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.

Author: John R. Dean
Publisher: John Wiley & Sons
ISBN: 0470861320
Category : Science
Languages : en
Pages : 284

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Book Description
Provides the basic skills and information required to prepare an environmental sample for analysis. Divided into two sections, i.e. Inorganic Analysis and Organic Analysis, this book covers selected techniques, principally atomic spectroscopy and chromatography. Using flow diagrams to augment the experimental information, it highlights the most appropriate methods and the likely results. Detailed experimental information provided in an easy-to-follow style with illustrations Describes the specific sample preparation approaches necessary to analyse a particular sample type Discussion of selected literature sources highlights the most appropriate methods and the likely results obtained

Author: Thomas R. Dulski
Publisher: CRC Press
ISBN: 9780824719852
Category : Technology & Engineering
Languages : en
Pages : 602

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Book Description
This work details minor, trace and ultratrace methods; addresses the essential stages that precede measurement; and highlights the measurement systems most likey to be used by the pragmatic analyst. It features key material on inclusion and phase isolation. The book is designed to provide useful maps and signposts for metals analysts who must verify that stringent trace level compositional specifications have been met.

Author: I.S. Krull
Publisher: Elsevier
ISBN: 0080858546
Category : Science
Languages : en
Pages : 319

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Book Description
The aim of this volume is to describe the most recent advances in areas of analytical chemistry that relate to the trace determination of metals and inorganics, as well as their distribution and forms (species) present, sample dependent. Analytical approaches are described that encompass a number of separation methods, such as gas and high performance liquid chromatography, interfaced with selective and sensitive detection methods that become unique for metal species/forms present in various samples. Hyphenated techniques are emphasized, such as interfacing HPLC with plasma induced emission spectroscopy, electrochemistry, post-column reaction chemistry, etc. Each chapter describes the latest instrumental and methodology advances that utilize some form of chromatography together with element-specific detection or mass spectrometry to provide absolute identification of the specific species of a metal present in various samples. The book will be of value to those concerned with the determination of trace levels of individual metal species present or suspected present in any given sample and to those involved in trace metal toxicology, metabolism of metal-containing drugs or chemicals, environmental exposures to metals and chemical speciation of real world samples. Government regulatory laboratories striving to detect and determine absolute levels of a metal species in any regulated sample will be interested in this volume, as will academic institutes involved in environmental toxicology, environmental chemistry, metal-DNA/protein interactions and researchers working with metal species.

Author: Erico Marlon Moraes Flores
Publisher: Elsevier
ISBN: 0128183489
Category : Science
Languages : en
Pages : 450

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Book Description
Microwave-Assisted Sample Preparation for Trace Element Analysis, Second Edition, describes the principles, equipment, and applications involved in sample preparation with microwaves for detecting and analyzing trace elements. Hot topics such as sample preparation for speciation, metabolomics, and halogen determination, as well as the alternatives of sample preparation for special samples (for example, carbon nanotubes, polymers, petroleum products), are also discussed. This completely updated second edition covers all the new devices and more powerful systems that have emerged in the last several years, such as Ultrawave and Ultraclave systems. New challenges in the fields of geology, environmental and biological studies -for example, the need for further determination of rare earth elements and halogens - are currently only covered in scientific journals and not in a comprehensive way. This book offers a summary of the state-of-the-art ways to meet these challenges with microwave-assisted sample preparation. The only book to cover in depth the principles, equipment, and applications of microwave-assisted sample preparation Written by experts in the field who provide a comprehensive overview of the important concepts Introduces the latest devices and systems used for in microwave-assisted techniques, including Ultrawave and Ultraclave systems

Author: Zeev B. Alfassi
Publisher: John Wiley & Sons
ISBN: 3527615768
Category : Science
Languages : de
Pages : 622

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Book Description
The best way to determine trace elements! This easy-to-use handbook guides the reader through the maze of all modern analytical operations. Each method is described by an expert in the field. The book highlights the advantages and disadvantages of individual techniques and enables pharmacologists, environmentalists, material scientists, and food industry to select a judicious procedure for their trace element analysis.

Author: C. Vandecasteele
Publisher: John Wiley & Sons
ISBN: 9780471974451
Category : Science
Languages : en
Pages : 352

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Book Description
Spurenanalyse von den theoretischen Grundlagen über die apparative Ausrüstung bis zur Probenpräparation - dieses Buch bringt Ihr Wissen über ICP-MS, HPLC-AAS, HPLC-ICP-MS und konventionellere Methoden auf den aktuellsten Stand. Viele Illustrationen und Beispiele aus der Praxis - so der biologischen Analytik und der Analytik hochreiner Materialien - empfehlen das Buch besonders für fortgeschrittene Studenten und Graduierte.

Author: Richard G. Whitney
Publisher: Penn State University Press
ISBN:
Category : Science
Languages : en
Pages : 114

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Book Description
"This book is a practical, 'how-to-do-it' guide to sampling water and analyzing for metals from atomic no. 21 (scandium) to atomic no. 30 (zinc). The list of elements includes chromium, copper, nickel, and other potential hazards. Optical and electrochemical methods, neutron activation analysis, and chromatography are discussed." - Environmental Science & Technology

Author: Hugh A. McKenzie
Publisher: Elsevier Publishing Company
ISBN:
Category : Science
Languages : en
Pages : 812

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Book Description
The understanding of the functions of trace elements in metabolism, whether associated with microorganisms, plants or animals, has advanced considerably during the last twenty years. There are two main aspects of the importance of trace elements in biological materials: first, their toxic effects and secondly, the essential nature of some of the elements for normal growth and health. Research in trace elements and their essential role in biological processes has advanced through several stages, necessitating more and more effective methods of determination. Despite the marked improvements in methods of trace analysis during these twenty years, the ever increasing need for higher sensitivity to meet new demands has meant the greater need, not only for improving the limits of detection, but also for new standard reference materials, better sampling, better sample handling and better design of trace and ultra-trace analysis laboratories. This book focusses on all areas of trace element determination with detailed discussion on all major methods of analysis. Additionally, the determination of concentrations of major toxic and essential trace elements is discussed at length.