RMN de l'oxygène-17 et nouvelles méthodologies de RMN des solides appliquées à la caractérisation des matériaux phosphates PDF Download

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RMN de l'oxygène-17 et nouvelles méthodologies de RMN des solides appliquées à la caractérisation des matériaux phosphates

RMN de l'oxygène-17 et nouvelles méthodologies de RMN des solides appliquées à la caractérisation des matériaux phosphates PDF Author: Alexandrine Flambard
Publisher:
ISBN:
Category :
Languages : fr
Pages : 298

Book Description
Ce travail concerne l'étude des verres de phosphate par RMN du solide et principalement par RMN de l' oxygène-l7. D'abord, nous proposons une méthode d'enrichissement en 17O, basée sur un échange isotopique sous vapeur d'eau enrichie. Cette méthode permet d'enrichir en 17O aussi bien des composés phosphates que des composés oxydes. Puis, nous avons adapté le concept SPAM afin d'améliorer la sensibilité des spectres haute résolution 3Q- et SI -MAS en 17O des verres de niobiophosphate. La résolution des spectres RMN du 31P de niobiophosphates cristallisés est aussi améliorée par découplage de l'interaction J entre le 31P et le 93Nb Enfin, les verres du système xNb2O5-(100-x)NaPO3 ont été caractérisés par une approche RMN multi-nucléaire. Un changement structural observé entre 20 et 30% molaire de Nb2O5 explique l'évolution des propriétés optiques non-linéaires. Ces résultats confortent les études structurales réalisées à partir d'autres techniques spectroscopiques.

RMN de l'oxygène-17 et nouvelles méthodologies de RMN des solides appliquées à la caractérisation des matériaux phosphates

RMN de l'oxygène-17 et nouvelles méthodologies de RMN des solides appliquées à la caractérisation des matériaux phosphates PDF Author: Alexandrine Flambard
Publisher:
ISBN:
Category :
Languages : fr
Pages : 298

Book Description
Ce travail concerne l'étude des verres de phosphate par RMN du solide et principalement par RMN de l' oxygène-l7. D'abord, nous proposons une méthode d'enrichissement en 17O, basée sur un échange isotopique sous vapeur d'eau enrichie. Cette méthode permet d'enrichir en 17O aussi bien des composés phosphates que des composés oxydes. Puis, nous avons adapté le concept SPAM afin d'améliorer la sensibilité des spectres haute résolution 3Q- et SI -MAS en 17O des verres de niobiophosphate. La résolution des spectres RMN du 31P de niobiophosphates cristallisés est aussi améliorée par découplage de l'interaction J entre le 31P et le 93Nb Enfin, les verres du système xNb2O5-(100-x)NaPO3 ont été caractérisés par une approche RMN multi-nucléaire. Un changement structural observé entre 20 et 30% molaire de Nb2O5 explique l'évolution des propriétés optiques non-linéaires. Ces résultats confortent les études structurales réalisées à partir d'autres techniques spectroscopiques.

Model Cellulosic Surfaces

Model Cellulosic Surfaces PDF Author: Maren Roman
Publisher: OUP USA
ISBN: 9780841269651
Category : Science
Languages : en
Pages : 0

Book Description
This book provides an overview of the different methods of model cellulosic surface preparation and presents recent studies on the properties of these surfaces. The topics covered are considered relatively new and would serve as the launch pad for further research in this area.

Signal Treatment and Signal Analysis in NMR

Signal Treatment and Signal Analysis in NMR PDF Author: D.N. Rutledge
Publisher: Elsevier
ISBN: 0080541208
Category : Science
Languages : en
Pages : 567

Book Description
Signal analysis and signal treatment are integral parts of all types of Nuclear Magnetic Resonance. In the last ten years, much has been achieved in the development of dimensional spectra. At the same time new NMR techniques such as NMR Imaging and multidimensional spectroscopy have appeared, requiring entirely new methods of signal analysis. Up until now, most NMR texts and reference books limited their presentation of signal processing to a short introduction to the principles of the Fourier Transform, signal convolution, apodisation and noise reduction. To understand the mathematics of the newer signal processing techniques, it was necessary to go back to the primary references in NMR, chemometrics and mathematics journals. The objective of this book is to fill this void by presenting, in a single volume, both the theory and applications of most of these new techniques to Time-Domain, Frequency-Domain and Space-Domain NMR signals. Details are provided on many of the algorithms used and a companion CD-ROM is also included which contains some of the computer programs, either as source code or in executable form. Although it is aimed primarily at NMR users in the medical, industrial and academic fields, it should also interest chemometricians and programmers working with other techniques.

Soil Analysis

Soil Analysis PDF Author: J. Gautheyrou
Publisher: CRC Press
ISBN: 9789054107163
Category : Technology & Engineering
Languages : en
Pages : 514

Book Description
The objective of this book is to provide a better understanding of tools for soil analysis in order to use them more efficiently. It covers sampling problems as well as difficulties relating to actual analysis and quality control.

What is the Code of Conduct for Responsible Fisheries?

What is the Code of Conduct for Responsible Fisheries? PDF Author: Food and Agriculture Organization of the United Nations
Publisher: Food & Agriculture Org.
ISBN: 9789251045411
Category : Business & Economics
Languages : en
Pages : 20

Book Description
The actual Code of conduct is also available (1996) (ISBN 9251038341).

Flexoelectricity in Liquid Crystals

Flexoelectricity in Liquid Crystals PDF Author: Agnes Buka
Publisher: World Scientific
ISBN: 1848167997
Category : Science
Languages : en
Pages : 299

Book Description
The book intends to give a state-of-the-art overview of flexoelectricity, a linear physical coupling between mechanical (orientational) deformations and electric polarization, which is specific to systems with orientational order, such as liquid crystals. Chapters written by experts in the field shed light on theoretical as well as experimental aspects of research carried out since the discovery of flexoelectricity. Besides a common macroscopic (continuum) description the microscopic theory of flexoelectricity is also addressed. Electro-optic effects due to or modified by flexoelectricity as well as various (direct and indirect) measurement methods are discussed. Special emphasis is given to the role of flexoelectricity in pattern-forming instabilities. While the main focus of the book lies in flexoelectricity in nematic liquid crystals, peculiarities of other mesophases (bent-core systems, cholesterics, and smectics) are also reviewed. Flexoelectricity has relevance to biological (living) systems and can also offer possibilities for technical applications. The basics of these two interdisciplinary fields are also summarized.

Sea Plants

Sea Plants PDF Author:
Publisher: Elsevier
ISBN: 012408107X
Category : Science
Languages : en
Pages : 593

Book Description
Advances in Botanical Research publishes in-depth and up-to-date reviews on a wide range of topics in plant sciences. The series features several reviews by recognized experts on all aspects of plant genetics, biochemistry, cell biology, molecular biology, physiology and ecology. This thematic volume, number 71, features reviews on sea plants. Its chapters cover topics such as the role of algae in sustainability; the status of kelp exploitation and marine agronomy; potential applications for enzymatic recovery of metabolites from seaweeds; and many more. - Publishes in-depth and up-to-date reviews on a wide range of topics in plant sciences - Features a wide range of reviews by recognized experts on all aspects of plant genetics, biochemistry, cell biology, molecular biology, physiology, and ecology - Volume features reviews on sea plants

Aquaculture Development

Aquaculture Development PDF Author: Food and Agriculture Organization of the United Nations
Publisher: Food & Agriculture Org.
ISBN: 9789251039717
Category : Business & Economics
Languages : en
Pages : 52

Book Description
Provides annotations to the Principles of Article 9 of the Code of Conduct for Responsible Fisheries. These annotations are meant to serve as general guidance, and should be taken as suggestions or observations intended to assist those interested in identifying their own criteria and options for actions, as well as partners for collaboration, in support of sustainable aquaculture development.

Clay-containing Polymeric Nanocomposites

Clay-containing Polymeric Nanocomposites PDF Author: L. A. Utracki
Publisher: iSmithers Rapra Publishing
ISBN: 9781859574379
Category : Technology & Engineering
Languages : en
Pages : 464

Book Description
This is Part 1 of a two-part set. Part 2 ISBN is 1859574823

Modern Surface Organometallic Chemistry

Modern Surface Organometallic Chemistry PDF Author: Jean-Marie Basset
Publisher: Wiley-VCH
ISBN: 9783527319725
Category : Science
Languages : en
Pages : 725

Book Description
Covering everything from the basics to recent applications, this monograph represents an advanced overview of the field. Edited by internationally acclaimed experts respected throughout the community, the book is clearly divided into sections on fundamental and applied surface organometallic chemistry. Backed by numerous examples from the recent literature, this is a key reference for all chemists.