Quantifying Uncertainty in Analytical Measurement PDF Download

Author: Eurachem/CITAC Working Group
Publisher:
ISBN: 9780948926150
Category : Chemistry, Analytic
Languages : en
Pages : 120

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Author:
Publisher:
ISBN:
Category : Business & Economics
Languages : en
Pages : 268

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Book Description
Dedicated specifically to nuclear analytical techniques, this publication is intended to assist scientists using alpha, beta and gamma spectrometries, neutron activation and XRF analyses, and other nuclear analytical methods, in assessing and quantifying the sources of uncertainty in their daily measurements.

Author: Paul De Bièvre
Publisher: Springer Science & Business Media
ISBN: 3662051737
Category : Science
Languages : en
Pages : 294

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Book Description
It is now becoming recognized in the measurement community that it is as important to communicate the uncertainty related to a specific measurement as it is to report the measurement itself. Without knowing the uncertainty, it is impossible for the users of the result to know what confidence can be placed in it; it is also impossible to assess the comparability of different measurements of the same parameter. This volume collects 20 outstanding papers on the topic, mostly published from 1999-2002 in the journal "Accreditation and Quality Assurance." They provide the rationale for why it is important to evaluate and report the uncertainty of a result in a consistent manner. They also describe the concept of uncertainty, the methodology for evaluating uncertainty, and the advantages of using suitable reference materials. Finally, the benefits to both the analytical laboratory and the user of the results are considered.

Author: Barry N. Taylor
Publisher: DIANE Publishing
ISBN: 1437915566
Category : Science
Languages : en
Pages : 25

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Book Description
Results of measurements and conclusions derived from them constitute much of the technical information produced by the National Institute of Standards and Technology (NIST). In July 1992 the Director of NIST appointed an Ad Hoc Committee on Uncertainty Statements and charged it with recommending a policy on this important topic. The Committee concluded that the CIPM approach could be used to provide quantitative expression of measurement that would satisfy NIST¿s customers¿ requirements. NIST initially published a Technical Note on this issue in Jan. 1993. This 1994 edition addresses the most important questions raised by recipients concerning some of the points it addressed and some it did not. Illustrations.

Author: Max Feinberg
Publisher: John Wiley & Sons
ISBN: 3527845267
Category : Science
Languages : en
Pages : 341

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Book Description
Quantification, Validation and Uncertainty in Analytical Sciences Companion guide explaining all processes in measuring uncertainty in quantitative analytical results Quantification, Validation and Uncertainty in Analytical Sciences provides basic and expert knowledge by building on the sequence of operations starting from the quantification in analytical sciences by defining the analyte and linking it to the calibration function. Proposing a comprehensive approach to MU (Measurement Uncertainty) estimation, it empowers the reader to apply Method Accuracy Profile (MAP) efficiently as a statistical tool in measuring uncertainty. The text elucidates several examples and template worksheets explaining the theoretical aspects of the procedure and includes novel method validation procedures that can accurately estimate the data obtained in measurements. It also enables the reader to provide practical insights to improve decision making by accurately evaluating and comparing different analytical methods. Brings together an interdisciplinary approach with statistical tools and algorithms applied in analytical chemistry and written by two international experts with long-standing experience in the field of Analytical measurements and Uncertainty, Quantification, Validation and Uncertainty in Analytical Sciences includes information on: The know-how of methods in an analytical laboratory, effective usage of a spurious measurement and methods to estimate errors. Quantification, calibration, precision, trueness, MAP addons, estimating MU for analytical sciences, and uncertainty functions Employing measurement uncertainty, sampling uncertainty, quantification limits, and sample conformity assessment Decision making, uncertainty and standard addition method, and accuracy profile for method comparison Quantification, Validation and Uncertainty in Analytical Sciences is an ideal resource for every individual quantifying or studying analytes. With several chapters dedicated to MU’s practical use in decision making demonstrating its advantages, the book is primarily intended for professional analysts, although researchers and students will also find it of interest.

Author: Paolo Fornasini
Publisher: Springer Science & Business Media
ISBN: 0387786503
Category : Technology & Engineering
Languages : en
Pages : 291

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Book Description
The scienti c method is based on the measurement of di erent physical qu- tities and the search for relations between their values. All measured values of physical quantities are, however, a ected by uncertainty. Understanding the origin of uncertainty, evaluating its extent, and suitably taking it into account in data analysis, are fundamental steps for assessing the global accuracy of physical laws and the degree of reliability of their technological applications. The introduction to uncertainty evaluation and data analysis procedures is generally made in laboratory courses for freshmen. During my long-lasting teaching experience, I had the feeling of some sort of gap between the ava- able tutorial textbooks, and the specialized monographs. The present work aims at lling this gap, and has been tested and modi ed through a feedback interaction with my students for several years. I have tried to maintain as much as possible a tutorial approach, that, starting from a phenomenolo- cal introduction, progressively leads to an accurate de nition of uncertainty and to some of the most common procedures of data analysis, facilitating the access to advanced monographs. This book is mainly addressed to - dergraduate students, but can be a useful reference for researchers and for secondary school teachers. The book is divided into three parts and a series of appendices. Part I is devoted to a phenomenological introduction to measurement and uncertainty. In Chap.

Author:
Publisher:
ISBN: 9780948926129
Category : Chemistry, Analytic
Languages : en
Pages : 54

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Author: L. Kirkup
Publisher: Cambridge University Press
ISBN: 1139454900
Category : Science
Languages : en
Pages : 196

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Book Description
Measurement shapes scientific theories, characterises improvements in manufacturing processes and promotes efficient commerce. In concert with measurement is uncertainty, and students in science and engineering need to identify and quantify uncertainties in the measurements they make. This book introduces measurement and uncertainty to second and third year students of science and engineering. Its approach relies on the internationally recognised and recommended guidelines for calculating and expressing uncertainty (known by the acronym GUM). The statistics underpinning the methods are considered and worked examples and exercises are spread throughout the text. Detailed case studies based on typical undergraduate experiments are included to reinforce the principles described in the book. This guide is also useful to professionals in industry who are expected to know the contemporary methods in this increasingly important area. Additional online resources are available to support the book at www.cambridge.org/9780521605793.

Author: EURACHEM.
Publisher:
ISBN:
Category :
Languages : en
Pages : 120

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Author: Baptiste Gault
Publisher: Springer Science & Business Media
ISBN: 146143436X
Category : Technology & Engineering
Languages : en
Pages : 411

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Book Description
Atom probe microscopy enables the characterization of materials structure and chemistry in three dimensions with near-atomic resolution. This uniquely powerful technique has been subject to major instrumental advances over the last decade with the development of wide-field-of-view detectors and pulsed-laser-assisted evaporation that have significantly enhanced the instrument’s capabilities. The field is flourishing, and atom probe microscopy is being embraced as a mainstream characterization technique. This book covers all facets of atom probe microscopy—including field ion microscopy, field desorption microscopy and a strong emphasis on atom probe tomography. Atom Probe Microscopy is aimed at researchers of all experience levels. It will provide the beginner with the theoretical background and practical information necessary to investigate how materials work using atom probe microscopy techniques. This includes detailed explanations of the fundamentals and the instrumentation, contemporary specimen preparation techniques, experimental details, and an overview of the results that can be obtained. The book emphasizes processes for assessing data quality, and the proper implementation of advanced data mining algorithms. Those more experienced in the technique will benefit from the book as a single comprehensive source of indispensable reference information, tables and techniques. Both beginner and expert will value the way that Atom Probe Microscopy is set out in the context of materials science and engineering, and includes references to key recent research outcomes.