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Author: Frank Schneider Publisher: Springer Science & Business Media ISBN: 3709158273 Category : Science Languages : en Pages : 550
Book Description
The most important task of the analytical chemist, aside from the acquisition of experimental data, is the coordination and interpretation of such data in terms of the qualitative and quantitative composition of the test substance. As in the old tale of the blind men and the elephant, a single observation or test, not considered in conjunction with others, may lead to entirely erroneous conclusions. On the other hand, mere in crease in the number of such tests, without regard to their need or to their relationship to each other, also may not suffice for drawing the correct inferences from the experimental evidence. The deductive reasoning which is usually associated with the analy tical chemist finds its greatest opportunity for application in the problems of cognition and recognition of carbon compounds. Since a rigid scheme of procedure tends to produce a corresponding rigidity of thought, the intent of the present book is to outline approaches which will minimize the chances of misinterpretation without restricting the analytical chemist in his choice of tests. The selection of subsequent tests or reactions should be governed by the results of the preceding ones rather than by an arbi trary list. The relationships of the various approaches (and the information derived from each) to the composition and constitution of the test sub stance are brought out in the discussion with the hope that they may serve as guide lines for such selection.
Author: Frank Schneider Publisher: Springer Science & Business Media ISBN: 3709158273 Category : Science Languages : en Pages : 550
Book Description
The most important task of the analytical chemist, aside from the acquisition of experimental data, is the coordination and interpretation of such data in terms of the qualitative and quantitative composition of the test substance. As in the old tale of the blind men and the elephant, a single observation or test, not considered in conjunction with others, may lead to entirely erroneous conclusions. On the other hand, mere in crease in the number of such tests, without regard to their need or to their relationship to each other, also may not suffice for drawing the correct inferences from the experimental evidence. The deductive reasoning which is usually associated with the analy tical chemist finds its greatest opportunity for application in the problems of cognition and recognition of carbon compounds. Since a rigid scheme of procedure tends to produce a corresponding rigidity of thought, the intent of the present book is to outline approaches which will minimize the chances of misinterpretation without restricting the analytical chemist in his choice of tests. The selection of subsequent tests or reactions should be governed by the results of the preceding ones rather than by an arbi trary list. The relationships of the various approaches (and the information derived from each) to the composition and constitution of the test sub stance are brought out in the discussion with the hope that they may serve as guide lines for such selection.
Author: Al Steyermark Publisher: Elsevier ISBN: 0323161367 Category : Science Languages : en Pages : 684
Book Description
Quantitative Organic Microanalysis, Second Edition presents the recommendations of the American Chemical Society group for specification and methods of organic microanalysis. This book is organized into 23 chapters, and starts with discussions on test samples, blank tests, second type of efficient vibration-absorbing balance table, and microchemical balances. Other general topics covered include the Kjeldahl procedures to determine nitrogen compounds; oxygen flask combustions; determination of fluorine; and microhydrogenation. The final chapters present the modification of the procedure for the determination of oxygen using gravimetry. This book will be of great value to microanalysts, researchers, and college students who wants to expand their understanding in organic microanalysis.
Author: E. P. Clark Publisher: Elsevier ISBN: 1483275914 Category : Science Languages : en Pages : 144
Book Description
Semimicro Quantitative Organic Analysis focuses on the analytical phase of research and chemistry of natural products, as well as analysis of gases and methods used in identifying iodine and other substances. The manuscript first offers information on the determination of carbon, hydrogen, and nitrogen, and the use of Kjeldahl and Dumas methods in the determination of nitrogen. The book also ponders on the determination of halogens, including the use of ethanolamine-sodium, Carius, and sodium peroxide fusion methods and the Liepert volumetric method for iodine. The publication discusses the determination of sulfur and phosphorus, as well as the alkali-nitrate fusion method for converting organic phosphorus to orthophosphate and Woy's procedure for weighing phosphorus as phosphomolybdic anhydride. The text also reviews the determination of methoxyl and ethoxyl and acetyl groups; determination of neutralization equivalent and molecular weights; and determination of volatile fatty acids. The manuscript is a dependable reference for readers interested in the chemistry of natural products.
Author: United States. Environmental Protection Agency. Library Systems Branch Publisher: ISBN: Category : Environmental protection Languages : en Pages : 702
Author: L. Mázor Publisher: Elsevier ISBN: 1483160653 Category : Science Languages : en Pages : 292
Book Description
Analytical Chemistry of Organic Halogen Compounds presents the procedures applied in the analysis of organic halogen compounds. This book is composed of eight chapters that discuss the methods involved in the production and application of organic halogen compounds and in overcoming contamination problems caused by these compounds. After briefly dealing with the preparation, characteristics, and reactions of organic halogen compounds, this book goes on discussing the fundamental concepts of methods for the detection of halogens in organic compounds, namely, chlorine, bromine, iodine, and fluorine. The following chapter describes the characteristic features, advantages, and disadvantages of ultramicro and submicro chemical methods. A chapter also examines the qualitative and quantitative studies of organic halogen compounds based on the thermal and chemical stability of these compounds. The concluding chapters discuss the interference or interfering effects of halogens and their elimination in the determination of other elements. A list of physical constants of organic halogen compounds of general pharmaceutical and industrial significance is provided. This book is an ideal source for analytical chemists and other workers who are interested in the theoretical bases of the methods.
Author: F. Feigl Publisher: Elsevier ISBN: 0444597972 Category : Science Languages : en Pages : 797
Book Description
Covering all theoretical and practical aspects of the applications of spot tests to organic analysis, this book includes information on more than 900 tests. It continues to be an indispensable reference to organic and analytical chemists in academia and in industry.
Author: Miroslov Vecera Publisher: Springer Science & Business Media ISBN: 1468418335 Category : Science Languages : en Pages : 417
Book Description
The American edition of our monograph is not a mere translation of the Czech edition, which appeared some five years ago. We have had to respect the fact that even such a short period has sufficed for progress in this field, and that the field of application of methods of organic analysis has widened. We have therefore revised a number of chapters in Part 1, the general part of the monograph-mainly those devoted to chromatographic methods, which have been extended and complemented by methods of thin-layer chromatography and electrophoresis. The chapters on the theory of color reactions and on analytical literature have also been extended; the chapter on spectral methods has been extended by including the use of proton magnetic resonance in organic analysis, and the list of references has been enlarged by adding books of importance for organic analysis. In Part 2, the part dealing specifically with various elements and chemical groups, we have extended the chapters on solubility and on acids and bases. The methods for the detection and identification of given classes of compounds have also been supplemented by references to recent papers.
Author: Frank Schneider
Author: Frank Schneider
Author: Al Steyermark
Author: Fritz Pregl
Author: E. P. Clark
Author: United States. Environmental Protection Agency. Library Systems Branch
Author: Henry M. Leicester
Author: L. Mázor
Author: F. Feigl
Author: Arthur Israel Vogel
Author: Miroslov Vecera