Qualitative and Quantitative Electron-microprobe Analysis PDF Download

Author:
Publisher:
ISBN:
Category :
Languages : en
Pages :

View

Book Description

Author: Roger Theisen
Publisher: Springer Science & Business Media
ISBN: 366225106X
Category : Technology & Engineering
Languages : en
Pages : 173

View

Book Description

Author: S. J. B. Reed
Publisher: Cambridge University Press
ISBN: 113944638X
Category : Science
Languages : en
Pages : 232

View

Book Description
Originally published in 2005, this book covers the closely related techniques of electron microprobe analysis (EMPA) and scanning electron microscopy (SEM) specifically from a geological viewpoint. Topics discussed include: principles of electron-target interactions, electron beam instrumentation, X-ray spectrometry, general principles of SEM image formation, production of X-ray 'maps' showing elemental distributions, procedures for qualitative and quantitative X-ray analysis (both energy-dispersive and wavelength-dispersive), the use of both 'true' electron microprobes and SEMs fitted with X-ray spectrometers, and practical matters such as sample preparation and treatment of results. Throughout, there is an emphasis on geological aspects not mentioned in similar books aimed at a more general readership. The book avoids unnecessary technical detail in order to be easily accessible, and forms a comprehensive text on EMPA and SEM for geological postgraduate and postdoctoral researchers, as well as those working in industrial laboratories.

Author: S. J. B. Reed
Publisher: Cambridge University Press
ISBN: 9780521599443
Category : Science
Languages : en
Pages : 350

View

Book Description
This 1993 book gives a comprehensive account of both experimental and theoretical aspects of electron microprobe analysis, and is an extensively updated version of the seminal first edition, published in 1975. The design and operation of the instrument, including the electron column and both wavelength- and energy-dispersive X-ray spectrometers, are covered in the first part of the book. Experimental procedures for qualitative and quantitative analysis, using both types of spectrometer, are then discussed. Matrix ('ZAF') corrections, as required for quantitative analysis, are treated in some detail from both theoretical and practical viewpoints. Special considerations applying to the analysis of 'light' elements (atomic number below 10) are covered in a separate chapter. The emphasis throughout is on a sound understanding of principles and the treatment is applicable equally to the electron microprobe in its 'classical' form and to scanning electron microscopes fitted with X-ray spectrometers.

Author: K.F.J. Heinrich
Publisher: Springer Science & Business Media
ISBN: 0306438240
Category : Science
Languages : en
Pages : 412

View

Book Description
In 1968, the National Bureau of Standards (NBS) published Special Publication 298 "Quantitative Electron Probe Microanalysis," which contained proceedings of a seminar held on the subject at NBS in the summer of 1967. This publication received wide interest that continued through the years far beyond expectations. The present volume, also the result of a gathering of international experts, in 1988, at NBS (now the National Institute of Standards and Technology, NIST), is intended to fulfill the same purpose. After years of substantial agreement on the procedures of analysis and data evaluation, several sharply differentiated approaches have developed. These are described in this publi cation with all the details required for practical application. Neither the editors nor NIST wish to endorse any single approach. Rather, we hope that their exposition will stimulate the dialogue which is a prerequisite for technical progress. Additionally, it is expected that those active in research in electron probe microanalysis will appreciate more clearly the areas in which further investigations are warranted.

Author: K.F.J. Heinrich
Publisher: Springer Science & Business Media
ISBN: 1489926178
Category : Science
Languages : en
Pages : 397

View

Book Description
In 1968, the National Bureau of Standards (NBS) published Special Publication 298 "Quantitative Electron Probe Microanalysis," which contained proceedings of a seminar held on the subject at NBS in the summer of 1967. This publication received wide interest that continued through the years far beyond expectations. The present volume, also the result of a gathering of international experts, in 1988, at NBS (now the National Institute of Standards and Technology, NIST), is intended to fulfill the same purpose. After years of substantial agreement on the procedures of analysis and data evaluation, several sharply differentiated approaches have developed. These are described in this publi cation with all the details required for practical application. Neither the editors nor NIST wish to endorse any single approach. Rather, we hope that their exposition will stimulate the dialogue which is a prerequisite for technical progress. Additionally, it is expected that those active in research in electron probe microanalysis will appreciate more clearly the areas in which further investigations are warranted.

Author: A. J. Tousimis
Publisher:
ISBN:
Category : Electron probe microanalysis
Languages : en
Pages : 472

View

Book Description

Author: James Harold Moss
Publisher:
ISBN:
Category :
Languages : en
Pages : 226

View

Book Description

Author: Peter Ingram
Publisher: Academic Press
ISBN: 0080524567
Category : Science
Languages : en
Pages : 573

View

Book Description
Biomedical Applications of Microprobe Analysis is a combination reference/laboratory manual for the use of microprobe analysis in both clinical diagnostic and research settings. Also called microchemical microscopy, microprobe analysis uses high-energy bombardment of cells and tissue, in combination with high resolution EM or confocal microscopy to provide a profile of the ion, metal, and mineral concentrations present in a sample. This allows insight into the physiology and pathophysiology of a wide variety of cells and tissues.This book describes methods for obtaining detailed information about the identity and composition of particles too small to be seen with the naked eye and describes how this information can be useful in diagnostic and biomedical research. Up-to-date review of electron microprobe analysis Detailed descriptions of sample preparation techniques Recent technologies including confocal microscopy, infrared microspectroscopy, and laser raman spectroscopy Over 100 illustrations with numerous specific applications Contributions by world-renowned experts in the field Brief summary of highlights precedes each chapter

Author: E. Eichen
Publisher:
ISBN:
Category : Electron beams
Languages : en
Pages : 31

View

Book Description
The use of an electron microprobe as a research tool will be considered. The theory of operation of this instrument will be briefly discussed. The different possible modes of data presentation will be given. These will include graphical representation on a recorder, video representation of scanned area using backscattered electrons, absorbed electrons, and X-rays, and the accumulation of quantitative data on scalers. Qualitative, semiquantitative, and quantitative analysis will be included in the discussion. Also included will be the importance of specimen preparation in microprobe analysis, and a number of different examples for various types of specimens will be given. These will include such materials as metals, glasses, ceramics, and semiconductors. Consideration will be given to the analysis of thin films as well as bulk materials. Some of the problems encountered in the analysis of thin films will be discussed as well as ways of circumventing these problems. Examples will be given to illustrate the type of problems and the means of approach in cases where qualitative analysis, semiquantitative analysis, and quantitative analysis are desired. In the latter case, the different types of corrective procedures which can be used will be discussed. These include correction for absorption, fluorescence, and atomic number.