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Preparative Methods in Solid State Chemistry

Preparative Methods in Solid State Chemistry PDF Author: Paul Hagenmuller
Publisher: Elsevier
ISBN: 0323144365
Category : Science
Languages : en
Pages : 621

Book Description
Preparative Methods in Solid State Chemistry deals with the preparative methods used in solid state chemistry and highlights the importance of the chemist's role in preparing materials of desired quality as well as obtaining materials according to the requirements of the user such as the physicist. Topics covered range from high-pressure techniques in preparative chemistry to methods of growing single crystals of high-melting-point oxides. This book is comprised of 14 chapters and begins with an overview of possibilities for high-pressure synthesis, as well as the methods used to obtain high pressures, including transmission by gaseous or liquid fluids or in the solid state. The method of shock waves is then considered both from the point of view of thermodynamics and thermoelasticity, along with the possibility of using superpressures for evidently revolutionary applications. Subsequent chapters focus on the synthesis of single crystals of refractory oxides either at high temperatures (essentially liquid-solid transformations) or at lower temperatures in the presence of a solvent or a chemical reagent. The production of single crystals by electrolytic reduction in molten salts is also described. Numerous examples of vapor transport reactions in a temperature gradient are presented. This monograph should be of interest to chemists and students of solid state chemistry.

Preparative Methods in Solid State Chemistry

Preparative Methods in Solid State Chemistry PDF Author: Paul Hagenmuller
Publisher: Elsevier
ISBN: 0323144365
Category : Science
Languages : en
Pages : 621

Book Description
Preparative Methods in Solid State Chemistry deals with the preparative methods used in solid state chemistry and highlights the importance of the chemist's role in preparing materials of desired quality as well as obtaining materials according to the requirements of the user such as the physicist. Topics covered range from high-pressure techniques in preparative chemistry to methods of growing single crystals of high-melting-point oxides. This book is comprised of 14 chapters and begins with an overview of possibilities for high-pressure synthesis, as well as the methods used to obtain high pressures, including transmission by gaseous or liquid fluids or in the solid state. The method of shock waves is then considered both from the point of view of thermodynamics and thermoelasticity, along with the possibility of using superpressures for evidently revolutionary applications. Subsequent chapters focus on the synthesis of single crystals of refractory oxides either at high temperatures (essentially liquid-solid transformations) or at lower temperatures in the presence of a solvent or a chemical reagent. The production of single crystals by electrolytic reduction in molten salts is also described. Numerous examples of vapor transport reactions in a temperature gradient are presented. This monograph should be of interest to chemists and students of solid state chemistry.

Solid State Chemistry

Solid State Chemistry PDF Author: Lesley E. Smart
Publisher: CRC Press
ISBN: 1439847924
Category : Science
Languages : en
Pages : 483

Book Description
Building a foundation with a thorough description of crystalline structures, Solid State Chemistry: An Introduction, Fourth Edition presents a wide range of the synthetic and physical techniques used to prepare and characterize solids. Going beyond basic science, the book explains and analyzes modern techniques and areas of research. The book covers: A range of synthetic and physical techniques used to prepare and characterize solids Bonding, superconductivity, and electrochemical, magnetic, optical, and conductive properties STEM, ionic conductivity, nanotubes and related structures such as graphene, metal organic frameworks, and FeAs superconductors Biological systems in synthesis, solid state modeling, and metamaterials This largely nonmathematical introduction to solid state chemistry includes basic crystallography and structure determination, as well as practical examples of applications and modern developments to offer students the opportunity to apply their knowledge in real-life situations and serve them well throughout their degree course. New in the Fourth Edition Coverage of multiferroics, graphene, and iron-based high temperature superconductors, the techniques available with synchrotron radiation, and metal organic frameworks (MOFs) More space devoted to electron microscopy and preparative methods New discussion of conducting polymers in the expanded section on carbon nanoscience

New Directions in Solid State Chemistry

New Directions in Solid State Chemistry PDF Author: Chintamani Nagesa Ramachandra Rao
Publisher: Cambridge University Press
ISBN: 9780521301923
Category : Technology & Engineering
Languages : en
Pages : 528

Book Description
This book presents the highlights of modern solid state chemistry, an emerging area of chemical science. In adopting a unified and up-to-date approach the authors take the reader to the very frontiers of the subject, which is concerned primarily with new methods of synthesis, identification and characterization of solids, and above all with new strategies for tailor-making materials with desirable and controllable properties. The eight chapters are devoted to structure, methods of characterization, preparative strategies, phase transitions, defects and non-stoichiometry, structure-property relations, materials design, and reactivity of solids. Each of these reflects the way solid state chemistry is growing today and brings out the flavour of the subject to show how it works. In addition, every chapter ends with a list of important references.

Synthesis Methods and Crystallization

Synthesis Methods and Crystallization PDF Author: Riadh Marzouki
Publisher: BoD – Books on Demand
ISBN: 1838802231
Category : Technology & Engineering
Languages : en
Pages : 138

Book Description
New crystalline materials (organic, inorganic, hybrid) are promising for various applications, including electrical, piezoelectric, ferroelectric, magnetic, and catalytic processes. In addition, given their remarkable structural richness, these materials exhibit several interesting physical properties, such as ionic conduction, ion exchange, and others. Crystal growth, morphology, and grain size are factors influencing these physical properties. This book examines methods of synthesis of the most common crystalline materials and describes nucleation and crystal growth of various materials.

Handbook of Solid State Chemistry, 6 Volume Set

Handbook of Solid State Chemistry, 6 Volume Set PDF Author: Richard Dronskowski
Publisher: John Wiley & Sons
ISBN: 3527325875
Category : Technology & Engineering
Languages : en
Pages : 3912

Book Description
This most comprehensive and unrivaled compendium in the field provides an up-to-date account of the chemistry of solids, nanoparticles and hybrid materials. Following a valuable introductory chapter reviewing important synthesis techniques, the handbook presents a series of contributions by about 150 international leading experts -- the "Who's Who" of solid state science. Clearly structured, in six volumes it collates the knowledge available on solid state chemistry, starting from the synthesis, and modern methods of structure determination. Understanding and measuring the physical properties of bulk solids and the theoretical basis of modern computational treatments of solids are given ample space, as are such modern trends as nanoparticles, surface properties and heterogeneous catalysis. Emphasis is placed throughout not only on the design and structure of solids but also on practical applications of these novel materials in real chemical situations.

Solid State Chemistry and Its Applications

Solid State Chemistry and Its Applications PDF Author: Anthony R. West
Publisher: John Wiley & Sons
ISBN: 9780471908746
Category : Science
Languages : en
Pages : 752

Book Description
The first broad account offering a non-mathematical, unified treatment of solid state chemistry. Describes synthetic methods, X-ray diffraction, principles of inorganic crystal structures, crystal chemistry and bonding in solids; phase diagrams of 1, 2 and 3 component systems; the electrical, magnetic, and optical properties of solids; three groups of industrially important inorganic solids--glass, cement, and refractories; and certain aspects of organic solid state chemistry, including the ``organic metal'' of new materials.

Solid State Chemistry

Solid State Chemistry PDF Author: A. K. Cheetham
Publisher: Oxford University Press, USA
ISBN:
Category : Language Arts & Disciplines
Languages : en
Pages : 424

Book Description
This volume concentrates on methods for preparing solids and studying their stuctures and physical properties. A further volume will survey compounds with particularly important or useful properties.

Solid State Chemistry

Solid State Chemistry PDF Author: Aaron Wold
Publisher: Springer Science & Business Media
ISBN: 9401114765
Category : Science
Languages : en
Pages : 250

Book Description
The subject matterofsolid state chemistry lies within the spheres ofboth physical and inorganic chemistry. In addition, there is a large overlap with solid state physics and materials engineering. However, solid state chemistry has still to be recognized by the general body ofchemists as a legitimate subfield ofchemistry. The discipline is not even well defined as to content and has many facets that make writing a textbook a formidable task. The early studies carried out in the United States by Roland Ward and his co workers emphasized the synthesisofnew materials and the determination oftheir structure. His work on doped alkaline earth sulfides formed the basis for the development of infrared phosphors and his pioneering studies on oxides were important in understanding the structural features of both the perovskite oxides as well as the magnetoplumbites. In 1945, A. F. Wells published the first edition of Structural Inorganic Chemistry. This work attempts to demonstrate that the synthesis, structure, and properties of solids form an important part of inorganic chemistry. Now, after almost 50 years during which many notable advances have been made in solid state chemistry, it is still evident that the synthesis, structure determination, and properties of solids receive little attention in most treatments of inorganic chemistry. The development of the field since the early studies of Roland Ward (early 1940s) has been rapid.

New Directions in Solid State Chemistry

New Directions in Solid State Chemistry PDF Author: C. N. R. Rao
Publisher: Cambridge University Press
ISBN: 9780521499071
Category : Science
Languages : en
Pages : 568

Book Description
In the new edition of this widely praised textbook, all the chapters have been revised and the authors have brought the work completely up to date by the addition of new material on numerous topics. In recent years, solid state chemistry has emerged as a very important element of mainstream chemistry and materials science. Students, teachers and researchers need to understand the chemistry of solids because of the crucial role this plays in determining the properties of materials. An understanding of solid state chemistry is also essential in materials design, and many fascinating relationships between the structure and properties of solids have been discovered by chemists. This text requires only an understanding of basic physics, chemistry and crystallography, and is enhanced with the most recent examples, case studies and references. It will be of value to advanced students and researchers studying solid state chemistry and materials science as a text and reference work.

Solid State Chemistry

Solid State Chemistry PDF Author: Lesley E. Smart
Publisher: CRC Press
ISBN: 9780748740680
Category : Science
Languages : en
Pages : 412

Book Description
Intended for first- and second-year undergraduates, this introduction to solid-state chemistry includes practical examples of applications and modern developments to offer students the opportunity to apply their knowledge in real-life situations. It aims to provide students with a thorough understanding of the traditional knowledge of crystal structures: lattices, unit cells, close packing, and octahedral and tetrahedral holes and their occupation by various ions in the well-known crystal structures. This descriptive work is augmented by free-electron and band theory. Links to other branches of chemistry and practical examples are emphasized, as are the links back to band theory and crystal structures. For this second edition, the book has been updated throughout and has two new chapters, one on X-ray diffraction techniques and another on solid-state preparative methods, as well as new sections on symmetry and ferroelectrics.