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Modern Techniques in High-Resolution FT-NMR

Modern Techniques in High-Resolution FT-NMR PDF Author: Narayanan Chandrakumar
Publisher: Springer Science & Business Media
ISBN: 1461246261
Category : Science
Languages : en
Pages : 396

Book Description
The magnetism of nuclear spin systems has proved an amazingly fertile ground for the creativity of researchers. This happy circumstance results from the triple benediction that nature appears to have bestowed on nuclear spins: they are sporting spies-being infinitely manipulable (one is even tempted to say malleable), not unduly coy in revealing their secrets, and having a whole treasure house of secrets to reveal in the first place. researcher with Since spin dynamics are now orchestrated by the NMR ever more subtle scores, it is important to be able to tune into the pro ceedings with precision, if one is to make sense of it at all. Fortunately, it is not terribly difficult to do so, since in many ways spin dynamics are the theoretician's dream come true: they are often finite dimensional and quite tractable with basic quantum mechanics, frequently allowing near exact treatments and readily testable predictions. This book was conceived two years ago, with the objective of providing a simple, consistent introduction to the description of the spin dynamics that one encounters in modern NMR experiments. We believed it was a good time to attempt this, since it was possible by then to give sufficiently general descriptions of powelful classes of new NMR experiments. The choice of experiments we discuss in detail is necessarily subjective, al though we hope to have given a flavor of most of the important classes of pulse sequences, including some surface coil imaging applications.

Modern Techniques in High-Resolution FT-NMR

Modern Techniques in High-Resolution FT-NMR PDF Author: Narayanan Chandrakumar
Publisher: Springer Science & Business Media
ISBN: 1461246261
Category : Science
Languages : en
Pages : 396

Book Description
The magnetism of nuclear spin systems has proved an amazingly fertile ground for the creativity of researchers. This happy circumstance results from the triple benediction that nature appears to have bestowed on nuclear spins: they are sporting spies-being infinitely manipulable (one is even tempted to say malleable), not unduly coy in revealing their secrets, and having a whole treasure house of secrets to reveal in the first place. researcher with Since spin dynamics are now orchestrated by the NMR ever more subtle scores, it is important to be able to tune into the pro ceedings with precision, if one is to make sense of it at all. Fortunately, it is not terribly difficult to do so, since in many ways spin dynamics are the theoretician's dream come true: they are often finite dimensional and quite tractable with basic quantum mechanics, frequently allowing near exact treatments and readily testable predictions. This book was conceived two years ago, with the objective of providing a simple, consistent introduction to the description of the spin dynamics that one encounters in modern NMR experiments. We believed it was a good time to attempt this, since it was possible by then to give sufficiently general descriptions of powelful classes of new NMR experiments. The choice of experiments we discuss in detail is necessarily subjective, al though we hope to have given a flavor of most of the important classes of pulse sequences, including some surface coil imaging applications.

Modern Techniques in High-Resolution FT-NMR

Modern Techniques in High-Resolution FT-NMR PDF Author: Narayanan Chandrakumar
Publisher:
ISBN: 9781461246275
Category :
Languages : en
Pages : 400

Book Description


Principles of High Resolution NMR in Solids

Principles of High Resolution NMR in Solids PDF Author: M. Mehring
Publisher: Springer Science & Business Media
ISBN: 3642687563
Category : Science
Languages : en
Pages : 352

Book Description
The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level. Unfortunately the high resolution achievable in liquid solutions could not be obtained in solids and physicists and physical chemists had to live with unresolved lines open to a wealth of curve fitting procedures and a vast amount of speculations. High resolution NMR in solids seemed to be a paradoxon. Broad structure less lines are usually encountered when dealing with NMR in solids. Only with the recent advent of mUltiple pulse, magic angle, cross-polarization, two-dimen sional and multiple-quantum spectroscopy and other techniques during the last decade it became possible to resolve finer details of nuclear spin interactions in solids. I have felt that graduate students, researchers and others beginning to get involved with these techniques needed a book which treats the principles, theo retical foundations and applications of these rather sophisticated experimental techniques. Therefore I wrote a monograph on the subject in 1976. Very soon new ideas led to the developement of "two-dimensional spectroscopy" and "multiple-quantum spectroscopy", topics which were not covered in the first edition of my book. Moreover an exponential growth of literature appeared in this area of research leaving the beginner in an awkward situation of tracing back from a current article to the roots of the experiment.

Pulse and Fourier Transform NMR

Pulse and Fourier Transform NMR PDF Author: Thomas C. Farrar
Publisher: Elsevier
ISBN: 0080918123
Category : Science
Languages : en
Pages : 132

Book Description
Pulse and Fourier Transform NMR: Introduction to Theory and Methods presents the different types of pulse experiments that are commonly used and provides the theoretical background necessary for understanding these techniques. This book evaluates the practical application of pulse methods and the necessary instrumentation. Organized into seven chapters, this book begins with an overview of the NMR fundamentals and the basic pulse methods. This text then summarizes the important features of pulse spectrometers. Other chapters consider the rationale, the advantages, and the limitations of Fourier transform NMR methods. This book discusses as well how the idea of the rotating frame can be utilized to understand certain experiments that extend the range of application of pulse methods. The final chapter deals with a few significant special uses of pulse techniques. This book is a valuable resource for chemists and readers who are familiar with high resolution NMR but with no background in pulse methods.

Perspectives in Modern Chemical Spectroscopy

Perspectives in Modern Chemical Spectroscopy PDF Author: David L. Andrews
Publisher: Springer Science & Business Media
ISBN: 3642754562
Category : Science
Languages : en
Pages : 333

Book Description
"An interesting and enlightening book well worth the time for someone who is grounded in the basics of spectroscopy, yet interested in newer techniques and applications... particularly useful in providing breadth for those whose work has caused them to narrow their appreciation of spectroscopy to one area." (Spectroscopy) "This book should be on the bookshelves of all chemists whose daily work involves the practical application of spectroscopy to chemical analysis." (Fresenius' J. of Analytical Chem.) "...stands in style between an introduction to the various topics covered and near monographic treatments...meets a real need." (Faraday Transactions) "It covers an enormous amount of spectral theory and methodology in a condensed and readable format." (SIM News)

Pulsed Magnetic Resonance

Pulsed Magnetic Resonance PDF Author: A. Abragam
Publisher: Oxford University Press
ISBN: 9780198539629
Category : Medical
Languages : en
Pages : 586

Book Description
This book is a tribute to E.L. Hahn, an outstanding physicist whose discovery of spin echoes and demonstration of nuclear free induction decay led to the most important methods of modern nuclear magnetic resonance. The wide impact of these methods in physics, chemistry, biology, and medicine is fully acknowledged. In addition, Hahn's fundamental contributions in nuclear quadrupole echo phenomena, level crossing techniques, self-induced transparency and laser physics have been of paramount importance. Reflecting the diversity of these key discoveries and their vital influence, the articles presented here offer a stimulating and challenging contribution to the scientific literature which will be read by students and research workers from the wide range of disciplines using NMR techniques.

Polymorphism in Pharmaceutical Solids

Polymorphism in Pharmaceutical Solids PDF Author: Harry G. Brittain
Publisher: CRC Press
ISBN: 1420073222
Category : Medical
Languages : en
Pages : 656

Book Description
Using clear and practical examples, Polymorphism of Pharmaceutical Solids, Second Edition presents a comprehensive examination of polymorphic behavior in pharmaceutical development that is ideal for pharmaceutical development scientists and graduate students in pharmaceutical science. This edition focuses on pharmaceutical aspects of polymorphism a

Multidimensional NMR Methods for the Solution State

Multidimensional NMR Methods for the Solution State PDF Author: Gareth A. Morris
Publisher: John Wiley & Sons
ISBN: 1118589084
Category : Science
Languages : en
Pages : 877

Book Description
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NOESY and TOSCY, and an account of the latest progress in the development of multidimensional techniques. This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here

Dynamic Modelling & Control of National Economies 1986

Dynamic Modelling & Control of National Economies 1986 PDF Author: B. Martos
Publisher: Elsevier
ISBN: 1483298124
Category : Business & Economics
Languages : en
Pages : 470

Book Description
This IFAC symposium considers the modelling, analysis and control of various economic and socio-economic systems. The volume is divided into three sections covering: economic theory; macroeconomic policymaking - national, sectoral and regional models; mathematical, algorithmical and computational methods of modelling, giving a clear and concise view of the use of computer systems in the world of economics.

Structure Elucidation by Modern NMR

Structure Elucidation by Modern NMR PDF Author: H. Duddeck
Publisher: Springer Science & Business Media
ISBN: 3642977812
Category : Science
Languages : en
Pages : 236

Book Description
For several years we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in the English version. This book could not have been written in the present form without the help of a number of col leagues and, therefore, we acknowledge gratefully the generous supply of samples from and useful discussions with B. Abegaz (Addis Ababa, Ethiopia), U.H. Brinker (Bingham, New York, USA), E.