Author: W. A. Spencer
Publisher:
ISBN:
Category :
Languages : en
Pages : 5
Book Description
As part of the Defense Programs Plant Directed Research and Development Program, the Savannah River Technology Center investigated the emerging area of miniature mass sensors for hydrogen and hydrogen isotope analysis. New sensors from Ferran Scientific and a beta prototype sensor from Mass Sensors, Inc. were purchased. A small pumping platform was designed and assembled. Components for miniature ion traps were investigated based on design information from Oak Ridge National Laboratories. The systems were compared to a conventional residual gas analyzer based on a Stanford Research RGA 300. Each of the sensors investigated had distinct advantages for particular applications. The Ferran system was the least expensive and the smallest, but it had low resolution for hydrogen and deuterium mixtures. The Mass Sensor unit used a new ExB design which achieved excellent resolution of the hydrogen isotopes in a small package. One limitation with the current design was the small 3 to 4 order dynamic range and another was a need for a variable sampling rate to speed analysis over a wider mass range.
Miniature Mass Spectrometers for Hydrogen Isotopic Analyses
Author: W. A. Spencer
Publisher:
ISBN:
Category :
Languages : en
Pages : 5
Book Description
As part of the Defense Programs Plant Directed Research and Development Program, the Savannah River Technology Center investigated the emerging area of miniature mass sensors for hydrogen and hydrogen isotope analysis. New sensors from Ferran Scientific and a beta prototype sensor from Mass Sensors, Inc. were purchased. A small pumping platform was designed and assembled. Components for miniature ion traps were investigated based on design information from Oak Ridge National Laboratories. The systems were compared to a conventional residual gas analyzer based on a Stanford Research RGA 300. Each of the sensors investigated had distinct advantages for particular applications. The Ferran system was the least expensive and the smallest, but it had low resolution for hydrogen and deuterium mixtures. The Mass Sensor unit used a new ExB design which achieved excellent resolution of the hydrogen isotopes in a small package. One limitation with the current design was the small 3 to 4 order dynamic range and another was a need for a variable sampling rate to speed analysis over a wider mass range.
Publisher:
ISBN:
Category :
Languages : en
Pages : 5
Book Description
As part of the Defense Programs Plant Directed Research and Development Program, the Savannah River Technology Center investigated the emerging area of miniature mass sensors for hydrogen and hydrogen isotope analysis. New sensors from Ferran Scientific and a beta prototype sensor from Mass Sensors, Inc. were purchased. A small pumping platform was designed and assembled. Components for miniature ion traps were investigated based on design information from Oak Ridge National Laboratories. The systems were compared to a conventional residual gas analyzer based on a Stanford Research RGA 300. Each of the sensors investigated had distinct advantages for particular applications. The Ferran system was the least expensive and the smallest, but it had low resolution for hydrogen and deuterium mixtures. The Mass Sensor unit used a new ExB design which achieved excellent resolution of the hydrogen isotopes in a small package. One limitation with the current design was the small 3 to 4 order dynamic range and another was a need for a variable sampling rate to speed analysis over a wider mass range.
A Mass Spectrometer for Routine Hydrogen Isotope Analysis
Author: C. M. Stevens
Publisher:
ISBN:
Category : Hydrogen
Languages : en
Pages : 16
Book Description
Publisher:
ISBN:
Category : Hydrogen
Languages : en
Pages : 16
Book Description
Mass Spectrometer for Accurate Hydrogen Isotopic Analyses
Author:
Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
A theoretical study of the mass spectrometric analysis of mixtures of the hydrogen and helium isotopes shows that mass discrimination and low ion intensity in ion sources are the principal factors that limit accuracy. A virtual-image ion source with short focal length and high brightness avoids these limitations. Suitable analyzers and accessory equipment are available. Development and construction of an ion source with the required characteristics are within the state of the art of mass spectrometry. A high-resolution mass spectrometer with a satisfactory ion source should routinely analyze mixtures of the hydrogen and helium isotopes accurately within +-0.5 percent relative (99.7 percent CL) with ordinary operating techniques. Isotopic equilibrium, auxiliary helium analyses, and accurate standard would not be needed. Analyses accurate within +-0.3 percent relative (99.7 percent CL) could be made by using accurately mixed standards.
Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
A theoretical study of the mass spectrometric analysis of mixtures of the hydrogen and helium isotopes shows that mass discrimination and low ion intensity in ion sources are the principal factors that limit accuracy. A virtual-image ion source with short focal length and high brightness avoids these limitations. Suitable analyzers and accessory equipment are available. Development and construction of an ion source with the required characteristics are within the state of the art of mass spectrometry. A high-resolution mass spectrometer with a satisfactory ion source should routinely analyze mixtures of the hydrogen and helium isotopes accurately within +-0.5 percent relative (99.7 percent CL) with ordinary operating techniques. Isotopic equilibrium, auxiliary helium analyses, and accurate standard would not be needed. Analyses accurate within +-0.3 percent relative (99.7 percent CL) could be made by using accurately mixed standards.
A Mass Spectrometer for Routine Hydrogen Isotope Analysis
Author: Alfred Otto Nier
Publisher:
ISBN:
Category : Hydrogen
Languages : en
Pages : 24
Book Description
Publisher:
ISBN:
Category : Hydrogen
Languages : en
Pages : 24
Book Description
A Mass Spectrometer for Routine Hydrogen Isotope Analyses
Advanced Mass Spectrometers for Hydrogen Isotope Analyses
Miniature Mass Spectrometers for Upper Atmosphere Composition Measurements
Author: A. D. Bailey
Publisher:
ISBN:
Category : Aerospace telemetry
Languages : en
Pages : 48
Book Description
A basic quadrupole mass spectrometer system for neutral and ionized gaseous composition measurements of the upper atmosphere is described. Emphasis is placed on the electronic circuits used with a particular miniature quadrupole rod assembly and ionizer. Circuits described include the power converter, scan waveform generator, dc and rf excitation generators, logarithmic output current amplifier, ion source filament emission regulator and signal-conditioning circuits for telemetering. A summary of performance specifications and critical design dimensions is included. (Author).
Publisher:
ISBN:
Category : Aerospace telemetry
Languages : en
Pages : 48
Book Description
A basic quadrupole mass spectrometer system for neutral and ionized gaseous composition measurements of the upper atmosphere is described. Emphasis is placed on the electronic circuits used with a particular miniature quadrupole rod assembly and ionizer. Circuits described include the power converter, scan waveform generator, dc and rf excitation generators, logarithmic output current amplifier, ion source filament emission regulator and signal-conditioning circuits for telemetering. A summary of performance specifications and critical design dimensions is included. (Author).
A Versatile Six-inch Radius Mass Spectrometer for Isotopic Analysis of Solids, Liquids, Or Gases
Author: H. O. Finley
Publisher:
ISBN:
Category : Isotopes
Languages : en
Pages : 80
Book Description
Publisher:
ISBN:
Category : Isotopes
Languages : en
Pages : 80
Book Description
Analytical Mass Spectrometry Section
Author: William R. Shields
Publisher:
ISBN:
Category : Mass spectrometry
Languages : en
Pages : 112
Book Description
Publisher:
ISBN:
Category : Mass spectrometry
Languages : en
Pages : 112
Book Description
Analytical Mass Spectrometry Section: Instrumentation and Procedures for Isotopic Analysis
Author: W. A. Shields
Publisher:
ISBN:
Category : Mass spectrometers
Languages : en
Pages : 112
Book Description
Publisher:
ISBN:
Category : Mass spectrometers
Languages : en
Pages : 112
Book Description