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High Resolution NMR in Solids Selective Averaging

High Resolution NMR in Solids Selective Averaging PDF Author: Ulrich Haeberlen
Publisher: Elsevier
ISBN: 0323160255
Category : Science
Languages : en
Pages : 205

Book Description
High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.

High Resolution NMR in Solids Selective Averaging

High Resolution NMR in Solids Selective Averaging PDF Author: Ulrich Haeberlen
Publisher: Elsevier
ISBN: 0323160255
Category : Science
Languages : en
Pages : 205

Book Description
High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.

High resolution NMR in solids

High resolution NMR in solids PDF Author:
Publisher:
ISBN:
Category : Magnetic resonance
Languages : en
Pages : 190

Book Description


High resolution NMR in solids

High resolution NMR in solids PDF Author:
Publisher:
ISBN:
Category :
Languages : en
Pages : 0

Book Description


High Resolution NMR

High Resolution NMR PDF Author: Edwin D. Becker
Publisher: Elsevier
ISBN: 0323161855
Category : Science
Languages : en
Pages : 369

Book Description
High Resolution NMR: Theory and Chemical Applications discusses the principles and theory of nuclear magnetic resonance and how this concept is used in the chemical sciences. This book is written at an intermediate level, with mathematics used to augment verbal descriptions of the phenomena. This text pays attention to developing and interrelating four approaches – the steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The style of this book is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. This book begins with a description of the basic physics, together with a brief account of the historical development of the field. It looks at the study of NMR in liquids, including high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. This book is intended to assist chemistry graduate students, advanced undergraduate students, or researchers to understand NMR at a fundamental level. This text also provides illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins.

Advances in Planar Lipid Bilayers and Liposomes

Advances in Planar Lipid Bilayers and Liposomes PDF Author: A. Leitmannova Liu
Publisher: Academic Press
ISBN: 0080554539
Category : Science
Languages : en
Pages : 283

Book Description
Advances in Planar Lipid Bilayers and Liposomes, Volume 6, continues to include invited chapters on a broad range of topics, covering both main arrangements of the reconstituted system, namely planar lipid bilayers and spherical liposomes. The invited authors present the latest results in this exciting multidisciplinary field of their own research group. Many of the contributors working in both fields over many decades were in close collaboration with the late Prof. H. Ti Tien, the founding editor of this book series. There are also chapters written by some of the younger generation of scientists included in this series. This volume keeps in mind the broader goal with both systems, planar lipid bilayers and spherical liposomes, which is the further development of this interdisciplinary field worldwide. - Contributions from newcomers and established and experienced researchers - Exploring theoretically and experimentally the planar lipid bilayer systems and spherical liposomes - This volume is dedicated to mark the Bilayer Lipid Membranes 45th anniversary

Annual Reports on NMR Spectroscopy

Annual Reports on NMR Spectroscopy PDF Author:
Publisher: Academic Press
ISBN: 0128209755
Category : Science
Languages : en
Pages : 422

Book Description
Annual Reports on NMR Spectroscopy, has established itself as a premier resource for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy. - Serves as the premier resource for learning the new techniques and applications of NMR spectroscopy - Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules - Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)

Principles of Magnetic Resonance

Principles of Magnetic Resonance PDF Author: Charles P. Slichter
Publisher: Springer Science & Business Media
ISBN: 366209441X
Category : Science
Languages : en
Pages : 662

Book Description
The first edition of this book was written in 1961 when I was Morris Loeb Lecturer in Physics at Harvard. In the preface I wrote: "The problem faced by a beginner today is enormous. If he attempts to read a current article, he often finds that the first paragraph refers to an earlier paper on which the whole article is based, and with which the author naturally assumes familiarity. That reference in turn is based on another, so the hapless student finds himself in a seemingly endless retreat. I have felt that graduate students or others beginning research in magnetic resonance needed a book which really went into the details of calculations, yet was aimed at the beginner rather than the expert. " The original goal was to treat only those topics that are essential to an understanding of the literature. Thus the goal was to be selective rather than comprehensive. With the passage of time, important new concepts were becoming so all-pervasive that I felt the need to add them. That led to the second edition, which Dr. Lotsch, Physics Editor of Springer-Verlag, encouraged me to write and which helped launch the Springer Series in Solid-State Sciences. Now, ten years later, that book (and its 1980 revised printing) is no longer available. Meanwhile, workers in magnetic resonance have continued to develop startling new insights.

Perspectives on Solid State NMR in Biology

Perspectives on Solid State NMR in Biology PDF Author: S.R. Kiihne
Publisher: Springer Science & Business Media
ISBN: 9401725799
Category : Science
Languages : en
Pages : 227

Book Description
Solid state NMR is rapidly emerging as a universally applicable method for the characterization of ordered structures that cannot be studied with solution methods or diffraction techniques. This proceedings -; from a recent international workshop - captures an image of the latest developments and future directions for solid state NMR in biological research, particularly on membrane proteins. Detailed information on how hormones or drugs bind to their membrane receptor targets is needed, e.g. for rational drug design. Higher fields are bringing clear improvements, and the power of solid state NMR techniques for studying amorphous and membrane associated peptides, proteins and complexes is shown by examples of applications at ultra-high fields. Progress in protein expression, experimental design and data analysis are also presented by leaders in these research areas.

New Techniques in Solid-State NMR

New Techniques in Solid-State NMR PDF Author: Jacek Klinowski
Publisher: Springer Science & Business Media
ISBN: 9783540221685
Category : Science
Languages : en
Pages : 372

Book Description
With contributions by numerous experts

Nuclear Magnetic Resonance of Liquid Crystals

Nuclear Magnetic Resonance of Liquid Crystals PDF Author: Ronald Y. Dong
Publisher: Springer Science & Business Media
ISBN: 1468402080
Category : Science
Languages : en
Pages : 268

Book Description
Liquid crystals have become ubiquitous in the displays for electronic devices, ranging from wrist watches to laptop computers. Nuclear magnetic resonance is one of the important mechanisms for determining their structures tures and properties. This book covers NMR techniques used in studying liquid crystals and present up to date results from such studies. Ronald Dong has worked on NMR in liquid crystals for much of his professional career. Topics covered include: Nuclear spin dynamics, orientational order, molecular field theories of liquid-crystal molecules, nuclear spin relaxation, spin relaxation, rotational and translational dynamics, internal dynamics of liquid-crystal molecules, NMR in liquid crystals; an appendix covers rotations, Euler angles and Wigner rotation matrices.