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Author: Thomas F. Degnan, Jr. Publisher: Wiley-Interscience ISBN: 9780471384168 Category : Technology & Engineering Languages : en Pages : 880
Book Description
Broad in scope, the Handbook of Experimental Catalysis describes the general theory and practice of using the Electron Capture Detector (ECD) to study reactions of thermal electrons with molecules. It reviews the electron affinities and thermodynamic and kinetic parameters of atoms, small molecules, and large organic molecules obtained by using various methods. Clearly written and organized, this book is a useful guide to both the theory and practice of experimental catalysis. In addition to information on the ECD, the book summarizes other methods for studying reactions of thermal electrons with molecules. It also discusses applications in analytical chemistry, physical chemistry, and biochemistry, and provides a data table of electron affinities. Analytical, physical, and environmental chemists, biochemists and biophysicists, and students in these disciplines will make good use of the Handbook of Experimental Catalysis in the study of these reactions.
Author: Thomas F. Degnan, Jr. Publisher: Wiley-Interscience ISBN: 9780471384168 Category : Technology & Engineering Languages : en Pages : 880
Book Description
Broad in scope, the Handbook of Experimental Catalysis describes the general theory and practice of using the Electron Capture Detector (ECD) to study reactions of thermal electrons with molecules. It reviews the electron affinities and thermodynamic and kinetic parameters of atoms, small molecules, and large organic molecules obtained by using various methods. Clearly written and organized, this book is a useful guide to both the theory and practice of experimental catalysis. In addition to information on the ECD, the book summarizes other methods for studying reactions of thermal electrons with molecules. It also discusses applications in analytical chemistry, physical chemistry, and biochemistry, and provides a data table of electron affinities. Analytical, physical, and environmental chemists, biochemists and biophysicists, and students in these disciplines will make good use of the Handbook of Experimental Catalysis in the study of these reactions.
Author: Shigeo Nishimura Publisher: Wiley-Interscience ISBN: Category : Science Languages : en Pages : 728
Book Description
A complete guide to the most important reduction method in organic synthesis The most comprehensive reference in the field, Handbook of Heterogeneous Catalytic Hydrogenation for Organic Synthesis provides synthetic chemists and chemical engineers in fine chemicals and pharmaceuticals with detailed experimental guidelines for heterogeneous catalytic hydrogenation. Organized by functional groups for ready reference and featuring detailed examples of hundreds of reactions, this handbook covers hydrogenations of alkenes, alkynes, aldehydes and ketones, nitriles, imines, nitro and nitroso compounds, carboxylic acids and esters, and aromatic and heterocyclic compounds. In addition, coverage includes the preparation of amines by reductive alkylation and the hydrogenolysis of a variety of compounds. Examples of hydrogenation of functional groups and reaction pathways are illustrated with numerous equations and schemes. Practitioners will appreciate the plenitude of experimental details given for most of the reactions selected, including amounts of reagents and catalysts, reaction temperatures, hydrogen pressures, and reaction times. They will also find helpful the more than one hundred tables included throughout the book detailing the effects of key factors governing rate and selectivity, such as compound structure, the nature of catalysts and supports, and the nature of solvents. Researchers will benefit from the introductory chapters covering an array of hydrogenation catalysts, including nickel, cobalt, copper, iron, platinum group metals, rhenium, and other oxide and sulfide catalysts, as well as reactors and reaction conditions.
Author: Meena Marafi Publisher: Elsevier ISBN: 0444638857 Category : Technology & Engineering Languages : en Pages : 470
Book Description
Handbook of Spent Hydroprocessing Catalysts, Second Edition, covers all aspects of spent hydroprocessing catalysts, both regenerable and non-regenerable. It contains detailed information on hazardous characteristics of spent and regenerated catalysts. The information forms a basis for determining processing options to make decisions on whether spent catalysts can be either reused on refinery site after regeneration or used as the source of new materials. For non-regenerable spent catalysts, attention is paid to safety and ecological implications of utilizing landfill and other waste handling and storage options to ensure environmental acceptance. As such, this handbook can be used as a benchmark document to develop threshold limits of regulated species. - Includes experimental results and testing protocols which serve as a basis for the development of methodologies for the characterization of solid wastes - Presents a database which assists researchers in selecting/designing research projects on spent catalysts, i.e., regeneration vs. rejuvenation and metal reclamation - Provides the environmental laws, acts, and liabilities to raise awareness in safety and health issues in all aspects of spent catalysts - Contains solid waste management procedures specific to hydroprocessing that serve as a model for designing research projects in other solid waste areas
Author: Joost Frenken Publisher: Springer ISBN: 3319444395 Category : Science Languages : en Pages : 232
Book Description
This book is devoted to the emerging field of techniques for visualizing atomic-scale properties of active catalysts under actual working conditions, i.e. high gas pressures and high temperatures. It explains how to understand these observations in terms of the surface structures and dynamics and their detailed interplay with the gas phase. This provides an important new link between fundamental surface physics and chemistry, and applied catalysis. The book explains the motivation and the necessity of operando studies, and positions these with respect to the more traditional low-pressure investigations on the one hand and the reality of industrial catalysis on the other. The last decade has witnessed a rapid development of new experimental and theoretical tools for operando studies of heterogeneous catalysis. The book has a strong emphasis on the new techniques and illustrates how the challenges introduced by the harsh, operando conditions are faced for each of these new tools. Therefore, one can also read this book as a collection of recipes for the development of operando instruments. At present, the number of scientific results obtained under operando conditions is still limited and mostly focused on a simple test reaction, the catalytic oxidation of CO. This reaction thus forms a natural binding element between the chapters, linking the demonstrations of new techniques, and also connecting the theoretical and experimental studies. Some first results on other reactions are also presented. If there is one thing that can be concluded already in this early stage, it is that the catalytic conditions themselves can have dramatic effects on the structure and composition of the surfaces of catalysts, which, in turn can greatly affect the mechanisms, the activity, and the selectivity of the chemical reactions that they catalyze.
Author: I. Chorkendorff Publisher: John Wiley & Sons ISBN: 3527605649 Category : Science Languages : en Pages : 469
Book Description
Until now, the literature has offered a rather limited approach to the use of fundamental kinetics and their application to catalytic reactions. Subsequently, this book spans the full range from fundamentals of kinetics and heterogeneous catalysis via modern experimental and theoretical results of model studies to their equivalent large-scale industrial production processes. The result is key knowledge for students at technical universities and professionals already working in industry. '... such an enterprise will be of great value to the community, to professionals as well as graduate and undergraduate students attempting to move into the field of modern catalysis and kinetics. I strongly recommend you publish this book based on the proposal.' - Prof. Dr. G. A. Samorjai, University of California 'Both authors are well respected specialists, with a very long record of original top-quality work and an international reputation. A book from these authors will be considered an authoritative piece of work, I definitely support this project and I am looking forward to use the book when published.' - Prof. Dr. D. E. Resasco, University of Oklahoma 'I wholly support the proposed project. The authors are very competent young colleagues and there is a real need for such a textbook' - Prof. Dr. G. Ertl, Fritz-Haber-Institut, Max-Planck-Gesellschaft, Berlin
Author: Gerhard Ertl Publisher: ISBN: Category : Heterogeneous catalysis Languages : en Pages : 504
Book Description
The first comprehensive survey of the principles and applications of heterogeneous catalysis! Starting with the invention of Döbereiner's tinder box and reaching importance with Haber's development of ammonia synthesis, heterogeneous catalysis has become a multi-billion dollar business. Simultaneously, literature on heterogeneous catalysis has become increasingly widespread and difficult to follow. This handbook collects the available knowledge on heterogeneous catalysis and provides the reader with easy-to-find yet comprehensive information. With contributions from more than 200 leading experts from all over the world it covers all aspects of the subject, from physico-chemical foundations to large-scale industrial applications. With its highly topical contributions, the straightforward presentation of the material and its comprehensive coverage, this handbook sets new standards. Saving you the time for laborious searches for information, it is an indispensable tool for every scientist working.
Author: M. Albert Vannice Publisher: Springer ISBN: 038728690X Category : Science Languages : en Pages : 97
Book Description
This manual of solutions to the problems in "Kinetics of Catalytic Reactions" has been prepared to assist those who use this book in a teaching function. However, these solutions should also benefit those outside the classroom who want to apply the principles and concepts that are discussed in the book. By studying and observing the approaches used in solving these problems, it is very likely that similar applications can be envisioned in different kinetic problems that the investigator might face. Thus the availability ofthese solutions is a good learning tool for everyone. Additional details and insight about the solutions provided can be obtained by reading the cited references. I have tried to eliminate all errors, both conceptual and typographical, in these solutions; however, the probability is high that I have not succeeded completely. Should any errors of commission (or omission) be found, I would greatly appreciate being informed. I can be reached at this email address: [email protected], or mail can be sent to me at: 107 Fenske Laboratory, Department of Chemical Engineering, The Pennsylvania State University, University Park, PA 16802. Albert Vannice v Contents Preface v Solutions to Problems Chapter 3 - Catalyst Characterization .
Author: Daniel Duprez Publisher: World Scientific ISBN: 1783263342 Category : Science Languages : en Pages : 1035
Book Description
This book offers a comprehensive overview of the most recent developments in both total oxidation and combustion and also in selective oxidation. For each topic, fundamental aspects are paralleled with industrial applications. The book covers oxidation catalysis, one of the major areas of industrial chemistry, outlining recent achievements, current challenges and future opportunities. One distinguishing feature of the book is the selection of arguments which are emblematic of current trends in the chemical industry, such as miniaturization, use of alternative, greener oxidants, and innovative systems for pollutant abatement. Topics outlined are described in terms of both catalyst and reaction chemistry, and also reactor and process technology.
Author: J. A. Dumesic Publisher: Wiley-VCH ISBN: Category : Language Arts & Disciplines Languages : en Pages : 340
Book Description
Defines the emerging field of catalytic reaction synthesis in the search for new catalysts and catalytic processes. Illustrates how experimental data from diverse sources can be consolidated to form a quantitative description of the essential chemistry taking place on the catalyst surface. Elucidates the possible relationships between catalyst kinetic properties and surface chemical bonding properties. Offers examples of microkinetic analysis and catalytic reaction synthesis for a variety of catalytic reactions over metals, oxides, and zeolite catalysts. Illustrates the underlying strategy used to formulate a microkinetic model, calibrate the model to the existing experimental data, and assess the critical aspects of the essential surface chemistry involved in the catalytic process.
Author: Thomas F. Degnan, Jr.
Author: Thomas F. Degnan, Jr.
Author: Shigeo Nishimura
Author: Robert Bernard Anderson
Author: Meena Marafi
Author: Joost Frenken
Author: I. Chorkendorff
Author: Gerhard Ertl
Author: M. Albert Vannice
Author: Daniel Duprez
Author: J. A. Dumesic