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Trace Metal Analysis and Speciation

Trace Metal Analysis and Speciation PDF Author: I.S. Krull
Publisher: Elsevier
ISBN: 0080858546
Category : Science
Languages : en
Pages : 319

Book Description
The aim of this volume is to describe the most recent advances in areas of analytical chemistry that relate to the trace determination of metals and inorganics, as well as their distribution and forms (species) present, sample dependent. Analytical approaches are described that encompass a number of separation methods, such as gas and high performance liquid chromatography, interfaced with selective and sensitive detection methods that become unique for metal species/forms present in various samples. Hyphenated techniques are emphasized, such as interfacing HPLC with plasma induced emission spectroscopy, electrochemistry, post-column reaction chemistry, etc. Each chapter describes the latest instrumental and methodology advances that utilize some form of chromatography together with element-specific detection or mass spectrometry to provide absolute identification of the specific species of a metal present in various samples. The book will be of value to those concerned with the determination of trace levels of individual metal species present or suspected present in any given sample and to those involved in trace metal toxicology, metabolism of metal-containing drugs or chemicals, environmental exposures to metals and chemical speciation of real world samples. Government regulatory laboratories striving to detect and determine absolute levels of a metal species in any regulated sample will be interested in this volume, as will academic institutes involved in environmental toxicology, environmental chemistry, metal-DNA/protein interactions and researchers working with metal species.

Trace Metal Analysis and Speciation

Trace Metal Analysis and Speciation PDF Author: I.S. Krull
Publisher: Elsevier
ISBN: 0080858546
Category : Science
Languages : en
Pages : 319

Book Description
The aim of this volume is to describe the most recent advances in areas of analytical chemistry that relate to the trace determination of metals and inorganics, as well as their distribution and forms (species) present, sample dependent. Analytical approaches are described that encompass a number of separation methods, such as gas and high performance liquid chromatography, interfaced with selective and sensitive detection methods that become unique for metal species/forms present in various samples. Hyphenated techniques are emphasized, such as interfacing HPLC with plasma induced emission spectroscopy, electrochemistry, post-column reaction chemistry, etc. Each chapter describes the latest instrumental and methodology advances that utilize some form of chromatography together with element-specific detection or mass spectrometry to provide absolute identification of the specific species of a metal present in various samples. The book will be of value to those concerned with the determination of trace levels of individual metal species present or suspected present in any given sample and to those involved in trace metal toxicology, metabolism of metal-containing drugs or chemicals, environmental exposures to metals and chemical speciation of real world samples. Government regulatory laboratories striving to detect and determine absolute levels of a metal species in any regulated sample will be interested in this volume, as will academic institutes involved in environmental toxicology, environmental chemistry, metal-DNA/protein interactions and researchers working with metal species.

Practical Gas Chromatography

Practical Gas Chromatography PDF Author: Katja Dettmer-Wilde
Publisher: Springer
ISBN: 3642546404
Category : Science
Languages : en
Pages : 904

Book Description
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Handbook of Natural Fibres

Handbook of Natural Fibres PDF Author: Ryszard M. Kozlowski
Publisher: Elsevier
ISBN: 0857095501
Category : Science
Languages : en
Pages : 649

Book Description
Growing awareness of environmental issues has led to increasing demand for goods produced from natural products, including natural fibres. The two-volume Handbook of natural fibres is an indispensible tool in understanding the diverse properties and applications of these important materials. Volume 1: Types, properties and factors affecting breeding and cultivation is an essential guide to a wide range of natural fibres, and highlights key techniques for their improvement.Part one reviews key types and fundamental properties of natural textile fibres. The production, identification and testing of a range of cotton, bast, silk and wool fibres are discussed, alongside bioengineered natural textile fibres. Part two goes on to explore the improvement of natural fibre properties and production through breeding and cultivation, beginning with a discussion of fibrous flax and cotton. Improved natural fibre production through the prevention of fungal growth is explored, along with the use of genetic engineering and biotechnology to enhance desirable characteristics. Finally, the wider impact of natural textile production is discussed, using wild silk enterprise programs as an example.With its distinguished editor and international team of expert contributors, the two volumes of the Handbook of natural fibres are essential texts for professionals and academics in textile science and technology. - Provides an essential guide to a wide range of natural fibres and highlights key techniques for their improvement - Reviews key types and fundamental properties of natural textile fibres, addressing the production, identification and testing of a range of cotton, bast, silk and wool fibres - Explores the improvement of natural fibre properties and production through breeding and cultivation, beginning with a discussion of fibrous flax and cotton

Inductively Coupled Plasmas in Analytical Atomic Spectrometry

Inductively Coupled Plasmas in Analytical Atomic Spectrometry PDF Author: Akbar Montaser
Publisher: John Wiley & Sons
ISBN: 0471188115
Category : Science
Languages : en
Pages : 1044

Book Description
The broadest source of information on analytical ICP spectrometry available in a coherent, single volume. Renowned contributors define theory, diagnostics, models, instrumentation and applications. They also discuss atomic emission, atomic fluorescence and mass spectrometries based on ICP sources for atomization, excitation and ionization. 'This book is HIGHLY RECOMMENDED.' Analytical Chemistry '... a handy reference for anyone attempting to understand the theory of ICPs and how they work. The detailed discussions of the various types of instrumentation and methods will be quite helpful to students and researchers in the field who want to broaden their understanding of analytical atomic spectroscopy.' Applied Spectroscopy '...Everyone involved in elemental analysis using ICP should have this book. It is useful for both experienced and novice ICP spectroscopists.' Spectroscopy

Analytical Atomic Spectrometry with Flames and Plasmas

Analytical Atomic Spectrometry with Flames and Plasmas PDF Author: José A. C. Broekaert
Publisher: John Wiley & Sons
ISBN: 3527606777
Category : Science
Languages : en
Pages : 432

Book Description
This completely revised second edition of the standard work has been expanded by some twenty percent to include more information on the latest developments and new apparatus. In particular, sections have been added on microplasmas and new types of spectrometers, while that on the rapidly expanding field of speciations with practical examples from life and environmental sciences have been included. Still in one handy volume, the book covers all the important modern aspects of atomic fluorescence, emission and absorption spectroscopy as well as plasma mass spectroscopy in a readily comprehensible and practice-oriented manner. A thorough explanation of the physical, theoretical and technical basics, example applications including the concrete execution of analysis and comprehensive cross-references to the latest literature allow even newcomers easy access to the methodologies described.

TRAC: Trends in Analytical Chemistry

TRAC: Trends in Analytical Chemistry PDF Author: U A Th Brinkman
Publisher: Elsevier
ISBN: 148327456X
Category : Science
Languages : en
Pages : 417

Book Description
TRAC: Trends in Analytical Chemistry, Volume 7 provides information pertinent to the trends in the field of analytical chemistry. This book discusses a variety of topics related to analytical chemistry, including biomolecular mass spectroscopy, affinity chromatography, electrochemical detection, nucleosides, and protein sequencing. Organized into 63 parts encompassing 158 chapters, this volume begins with an overview of the significance of quality and productivity in the analytical laboratory. This text then presents a comprehensive review on alcohol dehydrogenases, immobilization, and applications in analysis and synthesis. Other chapters consider the various tests for determining the excellence of quantitative assays available for analysts to utilize for method validation. This book discusses as well the primary challenge of neuropharmacologists to relate physiological functions to the many ligand binding sites identified in brain tissue. The final chapter deals with the fundamentals and applications of biosensors. This book is a valuable resource for analytical chemists, chemical engineers, clinical chemists, neuropharmacologists, and scientists.

Environmental Speciation and Monitoring Needs for Trace Metal-containing Substances from Energy-related Processes

Environmental Speciation and Monitoring Needs for Trace Metal-containing Substances from Energy-related Processes PDF Author:
Publisher:
ISBN:
Category : Energy facilities
Languages : en
Pages : 348

Book Description


Handbook of Spectroscopy

Handbook of Spectroscopy PDF Author: G¿nter Gauglitz
Publisher: John Wiley & Sons
ISBN: 3527321500
Category : Science
Languages : en
Pages : 2011

Book Description
This second, thoroughly revised, updated and enlarged edition provides a straightforward introduction to spectroscopy, showing what it can do and how it does it, together with a clear, integrated and objective account of the wealth of information that may be derived from spectra. It also features new chapters on spectroscopy in nano-dimensions, nano-optics, and polymer analysis. Clearly structured into sixteen sections, it covers everything from spectroscopy in nanodimensions to medicinal applications, spanning a wide range of the electromagnetic spectrum and the physical processes involved, from nuclear phenomena to molecular rotation processes. In addition, data tables provide a comparison of different methods in a standardized form, allowing readers to save valuable time in the decision process by avoiding wrong turns, and also help in selecting the instrumentation and performing the experiments. These four volumes are a must-have companion for daily use in every lab.

Sample Handling and Trace Analysis of Pollutants

Sample Handling and Trace Analysis of Pollutants PDF Author: Damia Barcelo
Publisher: Elsevier
ISBN: 0080540694
Category : Science
Languages : en
Pages : 1151

Book Description
This book is an updated, completely revised version of a previous volume in this series entitled: ENVIRONMENTAL ANALYSIS -- Techniques, applications and quality assurance. The book treats different aspects of environmental analysis such as sample handling and analytical techniques, the applications to trace analysis of pollutants (mainly organic compounds), and quality assurance aspects, including the use of certified reference materials for the quality control of the whole analytical process. New analytical techniques are presented that have been developed significantly over the last 6 years, like solid phase microextraction, microwave-assisted extraction, liquid chromatography-mass spectrometric methods, immunoassays, and biosensors. The book is divided into four sections. The first describes field sampling techniques and sample preparation in environmental matrices: water, soil, sediment and biota. The second section covers the application areas which are either based on techniques, like the use of gas chromatography-atomic emission detection, immunoassays, or coupled-column liquid chromatography, or on specific application areas, like chlorinated compounds, pesticides, phenols, mycotoxins, phytotoxins, radionuclides, industrial effluents and wastes, including mine waste. Validation and quality assurance are described in the third section, together with the interpretation of environmental data using advanced chemometric techniques. The final section reports the use of somewhat advanced analytical methods, usually more expensive, less routinely used or less developed, for the determination of pollutants.

An Introduction to Analytical Atomic Spectrometry

An Introduction to Analytical Atomic Spectrometry PDF Author: L. Ebdon
Publisher: John Wiley & Sons
ISBN: 9780471974185
Category : Science
Languages : en
Pages : 212

Book Description
Das umfassende Handbuch der Atomspektroskopie jetzt in sorgfältig überarbeiteter, noch besser organisierter zweiter Auflage! Ergänzt wurden Kapitel zu wichtigen neuen Verfahren wie der Plasma-Atomemissionsspektroskopie und der ICP-Massenspektrometrie. Fettgedruckte Stichworte, übersichtliche Diagramme und praktische Übungen erleichtern das Erarbeiten und Vertiefen des Stoffes. (02/98)