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Author: Jean-Nicolas Dumez Publisher: Royal Society of Chemistry ISBN: 1839168072 Category : Science Languages : en Pages : 505
Book Description
Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.
Author: Jean-Nicolas Dumez Publisher: Royal Society of Chemistry ISBN: 1839168072 Category : Science Languages : en Pages : 505
Book Description
Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.
Author: Karol Jackowski Publisher: Royal Society of Chemistry ISBN: 1782623817 Category : Medical Languages : en Pages : 419
Book Description
This book covers the recent NMR studies with the application of gaseous molecules. Among the comprehensively discussed aspects of the area it includes in particular: new multinuclear experiments that deliver spectral parameters of isolated molecules and provide the most accurate values of nuclear magnetic shielding, isotropic spin–spin coupling and relaxation times; advanced, precise and correct theoretical descriptions of spectral parameters of molecules as well as the application of gas-phase NMR measurements to chemical analysis and medicine. The progress of research in these fields is enormous and has rapidly changed our knowledge and understanding of molecular parameters in NMR spectroscopy. For example, accurate studies of the shielding for isolated molecules allow the exact determination of nuclear magnetic dipole moments, the calculated values of spectral parameters can be verified by precise gas-phase NMR measurements, and the application of hyperpolarized noble gases provides excellent MRI pictures of lungs. Aimed at graduates and researchers in spectroscopy, analytical chemistry and those researching the applications of NMR in medicine, this book presents the connections between sophisticated experiments, the theory of magnetic parameters and the exploration of new methods in practice.
Author: Jonathan Yong Publisher: Springer Nature ISBN: 3031466845 Category : Science Languages : en Pages : 307
Book Description
This book provides a comprehensive overview of Nuclear Magnetic Resonance (NMR) theory, its applications, and advanced techniques to improve the quality and speed of NMR data acquisition. In this book, the author expands his outstanding Ph.D. thesis and provides a valuable resource for researchers, professionals, and students in the field of NMR spectroscopy. The book covers quantum mechanics basics, and topics like density operators, pulse sequences, 1D pulse acquisition, INEPT (Insensitive nuclei enhancement by polarization transfer), product operators, and 2D NMR principles. It also explores innovative experiments like States HSQC (Heteronuclear Single Quantum Coherence) and echo-antiecho HSQC with gradients. In the subsequent chapters, the author discusses Pure Shift NMR, including PSYCHE (Pure Shift Yielded by Chirp Excitation) and its optimizations, such as waveform parameterization and time-reversal methods. The 'Discrete PSYCHE' approach and Ultrafast PSYCHE-iDOSY (Diffusion-ordered spectroscopy) are also highlighted. This book presents the POISE (Parameter Optimisation by Iterative Spectral Evaluation) software for real-time NMR experiment optimization, including pulse width calibration and Ernst angle optimization, and demonstrates applications across various NMR experiments. Lastly, the book examines accelerated 2D NMR data collection and the NOAH (NMR by Ordered Acquisition using 1H detection) supersequences, emphasizing automated pulse program creation using GENESIS (GENEration of Supersequences In Silico). Covered NMR experiments include 13C sensitivity-enhanced HSQC, 15N HMQC (Heteronuclear Multiple Quantum Coherence), dual HSQC, HSQC-TOCSY (Total Correlation Spectroscopy), HMBC (Heteronuclear Multiple Bond Correlation), and ADEQUATE (Adequate Sensitivity Double-Quantum Spectroscopy).
Author: Lizhi Xiao Publisher: Royal Society of Chemistry ISBN: 183916459X Category : Science Languages : en Pages : 626
Book Description
Describing comprehensively the development and applications of NMR to oil and gas exploration, this book will bring the literature up to date as it has developed very quickly in the last two decades. Outlining new methodologies, it will provide a thorough and comprehensive document enabling a better understanding of the basics of NMR physics, petrophysics, downhole tools and data interpretation. Written by an author with more than 30 years’ experience in this hot and important topic, this book is designed to meet the needs of the community and encourage applications in low field NMR.
Author: Piotr Garbacz Publisher: Royal Society of Chemistry ISBN: 1839169591 Category : Science Languages : en Pages : 268
Book Description
How can we study one of the most elusive molecular properties, chirality, using nuclear interactions with the magnetic field that are apparently insensitive to handedness? This book answers this question from the physicochemical point of view by providing a clear, coherent, and comprehensive review of methods used in NMR studies of chirality. Presented arguments based on fundamental physical and chemical laws and in-depth descriptions of new methods utilizing purely physical interactions are mainly addressed to spectroscopists in both academia and industry. The introductory chapters provide the reader with the basics of NMR spectroscopy as a tool for the study of chiral compounds, and those more interested in the methods of chiral discrimination will benefit from the brief description of their common points and reasons why some of them may or may not work. In the following chapters, the book shows rapid progress in a newly emerging field of chirality-sensitive NMR, in particular, a search for effects that give direct information about the absolute configuration of a molecule.
Author: Publisher: Elsevier ISBN: 0443295794 Category : Science Languages : en Pages : 208
Book Description
Annual Reports on NMR Spectroscopy, Volume 111 presents the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy. Chapters in this new release include Electrophoretic NMR, Traceability and uncertainty in NMR measurements, Quantitative NMR Spectroscopy, Advances in Non-Uniform Sampling NMR, NMR spectroscopy of natural and synthetic fibers, Characterization of transition alkane complexes, and Recent applications of low field NMR to membrane science. - Serves as the premier resource for learning new techniques and applications in NMR spectroscopy - Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules - Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)
Author: Paul Hodgkinson Publisher: Royal Society of Chemistry ISBN: 1788014197 Category : Science Languages : en Pages : 452
Book Description
Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. In this unique volume, a range of experts in different areas of modern solid-state NMR explain about their area of expertise, emphasising the “practical aspects” of implementing different techniques, and illustrating what questions can and cannot be addressed. Later chapters address complex materials, showing how different NMR techniques discussed in earlier chapters can be brought together to characterise important materials types. The volume as a whole focusses on topics relevant to the developing field of “NMR crystallography” – the use of solids NMR as a complement to diffraction crystallography. This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.
Author: John L. Markley Publisher: Oxford University Press ISBN: 0195094689 Category : Medical Languages : en Pages : 375
Book Description
This book presents a critical assessment of progress on the use of nuclear magnetic resonance spectroscopy to determine the structure of proteins, including brief reviews of the history of the field along with coverage of current clinical and in vivo applications. The book, in honor of Oleg Jardetsky, one of the pioneers of the field, is edited by two of the most highly respected investigators using NMR, and features contributions by most of the leading workers in the field. It will be valued as a landmark publication that presents the state-of-the-art perspectives regarding one of today's most important technologies.
Author: Navin Khaneja Publisher: Intechopen ISBN: 1838804196 Category : Science Languages : en Pages : 147
Book Description
Nuclear magnetic resonance (NMR) has evolved as a versatile tool in chemistry and biology. This scientific technique is based on the detection of magnetic moments of atomic nuclei arising due to an intrinsic property called spin because of their precession in static magnetic fields. Nuclei are excited by radio frequency (RF) magnetic fields and subsequently their precession is observed by the voltage they induce on an induction coil as they precess. In this book, we present some of the most exciting developments in the field of NMR: for example, new developments in NMR instrumentation, new magnet technology, RF coil design, the design of novel NMR sensors, and new developments of methods in solution and solid-state NMR These range from new methods for the fast acquisition of 2D spectrum to NMR studies of molecular interactions in ionic solutions. Solid-state methods for the analysis of polyvinyl chloride and NMR studies of torsion angles in polypeptides are also included. The book will be a useful reference for practitioners in the field and at the same time will appeal to a broad audience interested in the general area of NMR.
Author: Rongchun Zhang Publisher: Royal Society of Chemistry ISBN: 1788014006 Category : Science Languages : en Pages : 590
Book Description
Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.
Author: Jean-Nicolas Dumez
Author: Jean-Nicolas Dumez
Author: Karol Jackowski
Author: Jonathan Yong
Author: Lizhi Xiao
Author: Piotr Garbacz
Author: 
Author: Paul Hodgkinson
Author: John L. Markley
Author: Navin Khaneja
Author: Rongchun Zhang