Author: Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
ELECTRODEPOSITION OF PLUTONIUM FOR ALPHA PULSE HEIGHT ANALYSIS OF 236Pu IN 238Pu
Author: Nuclear Science Abstracts
Author: Proceedings of Environmental Plutonium Symposium, Held at LASL, August 4-5, 1971
Author: Eric B. FowlerPublisher:
ISBN:
Category : Plutonium
Languages : en
Pages : 132
Book Description
The Electrodeposition of Plutonium
Author: Oscar CookTentative Method for the Determination of Plutonium-239 and Plutonium-238 in Water (by a Coprecipitation Anion Exchange Technique).
Author: Publisher:
ISBN:
Category :
Languages : en
Pages : 20
Book Description
A procedure for the determination of plutonium 238 and plutonium 239 in water is described. The procedure consists of a coprecipitation, an anion exchange separation and electrodeposition, followed by alpha pulse height analysis. More specifically, the sample is acidified with nitric acid and plutonium-242 is added as a tracer before any chemical separations are performed. Iron is added to the water as iron (III) and the plutonium is coprecipitated with the iron as ferric hydroxide by adding ammonium hydroxide. After decantation and centrifugation, the ferric hydroxide precipitate containing the coprecipitated plutonium is dissolved and the solution is adjusted to 8M in HNO3 for anion exchange separation. When the sample fails to dissolve because of the presence of insoluble residue, the residue is treated by a rigorous acid dissolution using concentrated nitric acid and hydrofluoric acids. The sample is poured over an anion exchange column. The iron and most other elements that might be present pass through the column. Thorium is removed from the column with 12 M hydrochloric acid and then the plutonium is eluted by reducing it to plutonium (III) with the iodide ion. The plutonium is electrodeposited onto a stainless steel slide for counting by alpha pulse height analysis using a silicon surface barrier detector. From the recovery of the plutonium-242 tracer, the absolute amounts of plutonium-238 and plutonium-239 can be calculated, and from the volume of sample analyzed the concentrations of these two isotopes in the water sample can be calculated.
Users' Guides for Radioactivity Standards
Author: National Research Council (U.S.). Committee on Nuclear SciencePublisher: National Academies
ISBN:
Category : Radioactive substances
Languages : en
Pages : 96
Book Description
Rapid Methods for Measuring Radioactivity in the Environment
Author: Publisher:
ISBN:
Category : Environmental testing
Languages : en
Pages : 1090
Book Description
Plutonium Isotopes in the Environment
Author: Elis HolmAnnual Book of ASTM Standards
Author: ASTM InternationalPublisher:
ISBN:
Category : Materials
Languages : en
Pages : 1302
Book Description
Author: