Author: John Leonard Publisher: CRC Press ISBN: 9780748740710 Category : Science Languages : en Pages : 328
Book Description
The first edition of this book achieved considerable success due to its ease of use and practical approach, and to the clear writing style of the authors. The preparation of organic compounds is still central to many disciplines, from the most applied to the highly academic and, more tan ever is not limited to chemists. With an emphasis on the most up-to-date techniques commonly used in organic syntheses, this book draws on the extensive experience of the authors and their association with some of the world's mleading laboratories of synthetic organic chemistry. In this new edition, all the figures have been re-drawn to bring them up to the highest possible standard, and the text has been revised to bring it up to date. Written primarily for postgraduate, advanced undergraduate and industrial organic chemists, particularly those involved in pharmaceutical, agrochemical and other areas of fine chemical research, the book is also a source of reference for biochemists, biologists, genetic engineers, material scientists and polymer researchers.
Author: J.T. Sharp Publisher: Springer Science & Business Media ISBN: 9400908199 Category : Science Languages : en Pages : 212
Book Description
One of the very best things about organic chemistry is actually doing experimental work at the beneh. This applies not only at the profes sionallevel but also from the earliest stages of apprenticeship to the craft as a student. The fascination sterns from the nature of the sub ject itself, with its vast array of different types of reaction and its al most infinite variety of different chemical compounds. Each reaction and each new compound pose their own particular problems to chal lenge the skill and ingenuity of the chemist, whether working in a first-year teaching la bora tory or at the frontiers of research. This book is intended to provide basic guidance in the essential experimental techniques used in a typical undergraduate course. It gives concise coverage of the range of practical skills required, from first-year level when students may have no previous experience, up to final-year level when students are usually involved in more complex and dem an ding experimental work in supervised research projects. Our objective was to produce a handbook of techniques that could be used with a variety of practical courses throughout a student's whole period of study. Those who run practical courses generally have strong feelings about what particular experiments or exercises are appropriate for their own students, and it is rare that a book of experiments suitable for one department is acceptable to another.
Author: Stéphane Caron Publisher: John Wiley & Sons ISBN: 1118093569 Category : Science Languages : en Pages : 870
Book Description
A hands-on guide to assist in the planning and execution of synthetic reactions in the laboratory Despite the maturity of organic chemistry, it can still be very challenging to identify optimal methods for synthetic transformations that perform as well in real-world manufacturing processes as they do in the laboratory. This detailed and accessible guide attempts to address this vexing issue and deliver proven methodologies practicing synthetic chemists will find valuable for identifying reaction conditions that work reliably over the broadest possible range of substrates. Practical Synthetic Organic Chemistry: Provides a practical guide to strategically planning and executing chemical syntheses for the bench chemist in industry Discusses information that is not common knowledge beyond the boundaries of process chemistry groups, such as the synthetic routes of selected contemporary pharmaceutical drugs and practical solvents, as well as green chemistry concepts Highlights key reactions, including substitutions, additions, eliminations, rearrangements, oxidations, and reductions Addresses basic principles, mechanisms, advantages and disadvantages of the methodology, and techniques for achieving laboratory success Incorporating such an extraordinary wealth of information on organic chemistry and its related fields into one complete volume distinguishes Practical Synthetic Organic Chemistry as an incomparable desktop reference for professionals and an invaluable study aid for students.
Author: Reinhart Keese Publisher: John Wiley & Sons ISBN: 0470029668 Category : Science Languages : en Pages : 209
Book Description
Success in an experimental science such as chemistry depends on good laboratory practice, a knowledge of basic techniques, and the intelligent and careful handling of chemicals. Practical Organic Synthesis is a concise, useful guide to good laboratory practice in the organic chemistry lab with hints and tips on successful organic synthesis. Topics covered include: safety in the laboratory environmentally responsible handling of chemicals and solvents crystallisation distillation chromatographic methods extraction and work-up structure determination by spectroscopic methods searching the chemical literature laboratory notebooks writing a report hints on the synthesis of organic compounds disposal and destruction of dangerous materials drying and purifying solvents Practical Organic Synthesis is based on a successful course in basic organic chemistry laboratory practice which has run for several years at the ETH, Zurich and the University of Berne, and its course book Grundoperationen, now in its sixth edition. Condensing over 30 years of the authors’ organic laboratory teaching experience into one easy-to-read volume, Practical Organic Synthesis is an essential guide for those new to the organic chemistry laboratory, and a handy benchtop guide for practising organic chemists.
Author: Stéphane Caron Publisher: John Wiley & Sons ISBN: 1119448859 Category : Science Languages : de Pages : 850
Book Description
This book is a hands-on guide for the organic chemist. Focusing on the most reliable and useful reactions, the chapter authors provide the information necessary for a chemist to strategically plan a synthesis, as well as repeat the procedures in the laboratory. Consolidates all the key advances/concepts in one book, covering the most important reactions in organic chemistry, including substitutions, additions, eliminations, rearrangements, oxidations, reductions Highlights the most important reactions, addressing basic principles, advantages/disadvantages of the methodology, mechanism, and techniques for achieving laboratory success Features new content on recent advances in CH activation, photoredox and electrochemistry, continuous chemistry, and application of biocatalysis in synthesis Revamps chapters to include new and additional examples of chemistry that have been demonstrated at a practical scale
Author: Amrut Gaddamwar Publisher: GRIN Verlag ISBN: 3656420025 Category : Science Languages : en Pages : 212
Book Description
This book is designed to cover the “Basics principles of practical chemistry” Syllabus of M.Sc, B.Sc level courses and This book embodies eight chapters which are of basic importance in the curriculum of M.Sc chemistry students and provide a core course of organic chemistry, B.Sc for all branches of sciences. Each chapter consists of a methodical introduction, discussion of basic physicochemical principles involved and practical application & significances.Chapter on Organic synthesis contains Preparation of m-Dinitrobenzene, m-Nitroaniline, Hippuric Acid, Azlactone, phthalimide, 2, 4-Dihydroxyacetophenone,Anthracene-Maleicanhydrideadduct Microwave Assisted Synthesis of Aspirin, P-Bromoacetanilide,P-Bromoaniline 2, 4, 6 Tribromoaniline; 1, 3, 5 Tribromobenzene, Aspirin, Tetrahydrocarbazole, 7-Hydroxy4-Methyl Coumarin (Umbelliferon) and Synthesis of Phenyl Indole, 7 Hydroxy-3-Methyl Flavone, 2, 5 Di hydroxy Acetophenone, 4-Chloro Toluene, Benzilic Acid, Benzpinacol, 7-Hydroxy Coumarin, Maleic Anhydride, Benzophenone, Benzanilide, Caprolactam, Vanillyl Alcohol, Ortho and Para Nitro Phenols, Acridone.In chapter two consists of Isolation of Natural product such as Isolation of Piperine from Black-pepper, Caffeine from Tea Leaves, and Cineole from Eucalyptus Leaves. Chapter three is “Drug synthesis” it mainly contains synthesis of Paracetamol, Phenytoin, Benzocaine, Methyl Uracil, chlorbutol, Sulphanilamide, flourescein, Antipyrine Chapter four is Organic mixture analysis explained the binary as well as ternary mixture and solid- solid, solid-liquid, liquid-liquid types of mixture. While chapter five consists of spectral analysis in which UV, visible, NMR, IR etc and different types of chromatographic techniques. In chapter six Estimation of Mg+2 in Soil, Carbonates & Bicarbonates in soil, Ca2+ & Fe3+ in cement sample, Calcium in a Given Tablet and Determination of Chemical Oxygen Demand, Sodium, Potassium, Calcium, Li, Phosphorous In Human Serum, Manganese in Steel, Quinine, by flame photometry; Determination of Riboflavin by Flourometry, Blood Cholesterol by Colorimetry, Blood Glucose Colorimetry chapter seven consist of Assay of Ibuprofen, Analgin, Ascorbic Acid, Sulfanilamide, Riboflavin and Diazepam the last chapter is the “Advanced Applied analysis &Preparations” it consists of Preparation of Urea- Formaldehyde Resin, phenol-formaldehyde resin and Determinations of Acid value of Oil, Viscosity of lubricating oil, Zn2+ ions by complexometric titration.
Author: John Leonard
Author: J.T. Sharp
Author: Stéphane Caron
Author: Reinhart Keese
Author: T. Slater Price
Author: Stéphane Caron
Author: Thomas Slater Price
Author: Arthur I. Vogel
Author: Amrut Gaddamwar
Author: Lionel Guy Radcliffe